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y 1534 Willow Pass Road,Pinsburg,CA 94565-1701 <br /> ® MCCC7IYlpb@ll AnalyflCal. Inc. �up�lw�mcmpbefl.com/E77) .fflaa:mfii@mccmMbeH.wm <br /> 69 <br /> "When QuallI&Y Counts" <br /> Quality Control Report <br /> Client: Neil O.Anderson&Associates WorkOrder: 1403A85 <br /> Date Prepared: 3/28/14 BatchlD: 88743 <br /> Date Analyzed: 3/29/14 Extraction Method SW5030B <br /> Instrument: GC10 Analytical Method: SW8260B <br /> Matrix: Soil Unit: mg/Kg <br /> Project: #LZV 140001;NOA Drywell,Lodi,Ca Sample ID: MB/LCS-88743 <br /> 1403A66-004AMS/NISD <br /> QC Summary Report for SW8260B <br /> Analyte MS MSD SPK SPKRef MS MSD MSIMSD RPD RPD <br /> Result Result Val Val %REC %REC Limits Limit <br /> lert-Amyl methyl ether(TAME) 0.0403 0.04139 0.050 NO 80.6 82.8 70-130 2.67 30 <br /> Benzene 0.04519 0.04565 0.050 NO 90.4 91.3 70-130 1.01 30 <br /> t-Butyl alcohol(TBA) 0.1786 0.1732 0.20 NO 89.3 86.6 70-130 3.09 30 <br /> Chlorobenzene 0.04592 0.0462 0.050 NO 91.8 92.4 70-130 0.606 30 <br /> 1,2-Dibromoethane(EDB) 0.04535 0.04788 0.050 NO 90.7 95.8 70-130 5.44 30 <br /> 1,2-1)ichloroethane(1,2-DCA) 0.04141 0.04182 0.050 NO 82.8 83.6 70-130 0.987 30 <br /> 1,1-Dichloroethene 0.0347 0.03488 0.050 NO 69.4,F1 69.8,171 70-130 0.510 30 <br /> Diisopropyl ether(DIPE) 0.04183 0.04216 0.050 NO 83.7 84.3 70-130 0.775 30 <br /> Ethyl tert-butyl ether(ETBE) 0.04156 0.04272 0.050 NO 83.1 85.4 70-130 2.76 30 <br /> Methyl-t-butyl ether(MTBE) 0.04199 0.04324 0.050 NO 84 86.5 70-130 2.94 30 <br /> Toluene 0.04673 0.04789 0.050 NO 93.5 95.8 70-130 2.46 30 <br /> Trichloroethene 0.04544 0.04637 0.050 NO 90.9 92.7 70-130 2.01 30 <br /> Surrogate Recovery <br /> Dibromo8uoromethane 0.1683 0.1696 0.18 96 97 70-130 0.764 30 <br /> 1 Toluene-d8 0.1568 0.1583 0.18 90 90 70-130 0 30 <br /> 4-BFB 0.01648 0.01706 0.018 94 97 70-130 3.43 30 <br /> 1 <br /> CDPH ELAP 1144 NELAP 4033ORELAP QA/QC Officer <br /> Page 57 of 79 <br />