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© 1534 Willow Pass Road,Niubmg,CA 94565-1701 <br /> McCamgbell Analytical Inc. <br /> Toll Free Telephone:(877)252-9262/Fax(925)252-9269 <br /> "When Quality CO..IS° http://w .mccampbell.com/E-mad:..ffi@nccempb lR.c. <br /> Quality Control Report i <br /> Client: Neil O.Anderson&Associates WorkOrder: 1403A85 <br /> Date Prepared: 3/31/14 BatchlD: 88764 <br /> Date Analyzed: 3/29/14 Extraction Method SW5030B <br /> Instrument: GC28 Analytical Method. SW8260B <br /> Matrix: Water Unit: Rg/L <br /> Project: #LZV 140001;NOA Drywell,Lodi,Ca Sample ID: MB/LCS-88764 <br /> 1403A27-007BMS/MSD <br /> QC Summary Report for SW8260B <br /> Analyte MS MSD SPK SPKRef MS MSD MS/MSD RPD RPD <br /> Result Result Val Val %REC %REC Limits Limlt <br /> tert-Amyl methyl ether(TAME) 18.8 19.16 20 ND 94 95.8 70-130 1.88 20 <br /> Benzene 19.54 19.57 20 ND 97.7 97.9 70-130 0.187 20 <br /> t-Butyl alcohol(TBA) 71.69 78.2 80 ND 89.6 97.7 70-130 8.69 20 <br /> Chlorobenzene 19.45 19.61 20 ND 97.2 98.1 70-1300.851 20 <br /> 1,2-Dibromoethane(EDB) 19.79 19.98 20 ND 99 99.9 70-130 0.945 20 <br /> 1,2-Dichloroethane(1,2-DCA) 18.25 18.92 20 ND 91.3 94.6 70-130 3.61 20 <br /> 1,1-Dichloroethene 20.14 20.82 20 ND 101 104 70-130 3.34 20 <br /> Diisopropyl ether(DIPE) 20.07 20.03 20 ND 100 100 70-130 0 20 <br /> Ethyl tert-butyl ether(ETRE) 19.6 19.92 20 ND 98 99.6 70-130 1.62 20 <br /> Methyl-t-butyl ether(MTBE) 19.42 20.2 20 ND 97.1 101 70-130 3.97 20 <br /> Toluene 19.43 19.3 20 ND 97.2 96.5 70-130 0.659 20 <br /> Trichloroethene 18.7 18.83 20 ND 93.5 94.2 70-130 0.699 20 <br /> Surrogate Recovery <br /> Dibromofluoromethane 39.76 40.72 45 88 90 70-130 2.39 20 <br /> Toluene-d8 40.51 40.28 45 90 90 70-130 0 20 , <br /> 4-BFB 3.965 4.046 4.5 88 90 70-130 2.02 20 <br /> M <br /> I <br /> I <br /> CDPH ELAP 1644♦NELAP 4033ORELAP <br /> QA/QC Officer <br /> Page 60 of 7� <br />