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laboratories <br /> - ATC Associates, Inc <br /> ' 1117 Lone Palm Ave,Suite B Blank!QC Data <br /> Modesto, CA 95351 Method 8015M!8021 B!8260B <br /> Prol ID 54 62596 0001 Matrix Water <br /> Site Farmer Property <br /> Method Rep Lim <br /> ' Sample ID Blank Water Sod <br /> Units ug/L uga. mg/Kg <br /> Method 8015M 18021 B Date Analyzed 06/30/05 <br /> ' Total Petroleum Hydrocarbons <br /> @ Gasoline <50 50 10 <br /> Benzene <0 5 0 5 0 005 <br /> Toluene <0 5 0 5 0 005 <br /> Xylenes <1 0 10 0 010 <br /> Ethyi Benzene <0 5 0 5 0 005 <br /> ' Surrogate Spike Recovery 113% <br /> i <br /> Method 82608 Date Analyzed 06130/05 <br /> it-Butanol (TBA) <5 0 5 0 0 050 <br /> Methyl-t-Butyl Ether(MTBE) <0 5 0 5 0 005 <br /> NDi-Isopropyl Ether(DIPE) <0 5 0 5 0 005 <br /> Ethyl-t-Butyl Ether(ETBE) <0 5 0 5 0 005 <br /> t-Amyl Methyl Ether(TAME) <0 5 0 5 0 005 <br /> ' 1,2-Dichloroethane(1,2-DCA) <0 5 0 5 0005 <br /> 1,2-Dibromoethane(EDB) <0 5 0 5 0 005 <br /> i <br /> ' Surrogate Spike Recovery 92% <br /> Matrix Spike Recovery Summary <br /> Method Lab ID Client ID Analyte RPD <br /> RPD <br /> MS 1 MSD <br /> ' 8015M F06965 Effluent Gas 105 1 103 2 <br /> 8260E F06953 CMSD ETBE 1081111 3 <br /> Laboratory Control Spike Recovery Summary <br /> ' Method LCSID ID Analyte Percent <br /> Recovery <br /> ' 8021B LCS063OF Toluene 102 <br /> 8260B LCS063OF TAME 114 <br /> ' Note(s) <br /> Water samples are reported in ug[L soiVsludge samples m mgXg,productloNnon aqueous liquid samples in mg/L <br /> ND means not detected at or above the stated reporting limit NIA means analyte not applicable to this analysis <br /> ' 2905 R&rood Avenue Ceres CA 95307 e Phone (209) 581 -9280 • Fax (209) 581 -9282 <br /> email info@argonfcbs corn <br />