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laborataries <br /> t ATC Associates, Inc <br /> 1117 Lone Palm Ave, Suite B Blank 1 QC Data <br /> Modesto,CA 95351 Method 8015M 1802181 B260B <br /> Prol ID 54 62596 0001 Matnx Water <br /> Site Farmer Property <br /> Method Rep Lim <br /> Sample ID Blank - Water Sol] <br /> ' Units ug1L uglL mgJKg <br /> Method 8015M18021B Date Anal zed 04/15/05 <br /> Total Petroleum Hydrocarbons <br /> ' @ Gasoline <50 50 10 <br /> Benzene <0 5 0 5 0 005 <br /> Toluene <0 5 0 5 0 005 <br /> ' Xylenes <1 0 10 0 010 <br /> Ethyl Benzene <0 5 0 5 0 005 <br /> Surrogate Spike Recovery 104% <br /> Method 82808 Date Analyzed 04120105 <br /> ' t-Butanol(TBA) <50 5 0 0 050 <br /> Methykt-Butyl Ether(MTBE) <0 5 0 5 0 005 <br /> Di-Isopropyl Ether(RIPE) <0 5 0 5 0 005 <br /> Ethyl-t-Butyl Ether(ETBE) <0 5 0 5 0 005 <br /> t Amyl Methyl Ether(TAME) <0 5 0 5 0 005 <br /> 1,2-Dichloroethane(1,2-DCA) <0 5 0 5 0 005 <br /> ' 1,2-Dibromoethane(EDB) <05 0 5 0 005 <br /> Surrogate Spike Recovery 101% <br /> Matrix Spike Recovery Summary <br /> Method Lab ID Client ID Analyte %Recovery RPD <br /> MS 1 MSD <br /> ' 8015M F04235 MW5 Gas 86199 14 <br /> 8260B F04382 MW2 ETBE 1081111 3 <br /> ' LaboratoryControl Spike Recovery Summary <br /> ' Method _ LCSID ID Analyte Percent — <br /> Recovery <br /> 8021B LCSO415F2 o-Xylene 114 <br /> ' 8260B LCSO420F TAME 115 <br /> ' <br /> Note(s) <br /> Water samples are reported in ug]L soiUsludge samples in mglKg,producUoiVnon-aqueous liquid samples in mg1L <br /> . ND means not detected at or above the stated reporting limit NIA means analyte not applicable to this analysis <br /> 1 <br /> 2905 Po lroec l lvenue Ceres CR 95507 • ,phone (209) 581 -9280 s Lc)x (209) 58 1 -9282 <br /> ' emcll Info@orgonlobs com <br />