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i ANALYTICAL RESULTS Total Petroleum Hydrocarbons By GC WIin/GTEL Client ID CES06CES06 Number W1170118 Project ID (number) 97731 01 01 Method GC Project ID (name) FARMER PROPERTY/MODESTO/CA Matrix Solids ' NEI/GTEL Sample Number W7070068 11 W7070068-12 W7070068 13 W7070068 14 Client ID FP SB7 20 5 FP 567-25 5 FP-SB7 28 5 FP SB1 10 5 Date Sampled 07/01/97 07/01/97 07/01/97 06/30/97 Date Prepared 07/11/97 07/11/97 07/11/97 07/11/97 Date Analyzed 07/17/97 07/18/97 07/18/97 07/18/97 Dilution Factor 1 00 1 00 1 00 1 00 ' Reporting Analyte Limit Units Concentration Wet W_eig_ht TPH as Kerosene 10 mg/kg < 10 < 10 < 10 < 10 ' TPH as Diesel 10 mg/kg < 10 < 10 < 10 < 10 TPH as Lubricating Oil 10 mg/kg < 10 < 10 < 10 < 10 Percent Solids % 5B 0 79 1 81 1 76 4 Notes Dilution Factor Dilution factor indicates the adjustments made for sample dilution 'C Extraction by EPA Method 3550 (sonication) ASTM Method D3328(modified) is used for qualitative identification of fuel patterns The method has been j modified to include quantitation by applying calibration and quality assurance guidelines outlined in "Test Methods for Evaluating Solid Waste hysical/Chemical Methods' SW-846 Third Edition including promulgated Update 1 This method is equivalent to the California LOFT manual DHS method or diesel fuel Due to the qualitative similarities between Kerosene and Diesel Fuel the material present was quantified only as the product which it most resembled chromatographically The reporting limit for the other analyte was elevated accordingly Lubricating oil can not be qualitatively identified by type of oil because of chromatographic likeness of different oil types Due to non volatility of certain oils much of the oil present may not be quantified by this method Quantitation obtained for lubricating oil by this method should therefore be treated as an estimate This method quantifies lubricating oil against 10 W 30 standards 1 1 *I/GTEL Wichita KS ' W7070068 Page 2 I i