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GeoAnalytical Laboratories, Inc, <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209)572-0916 <br /> CERTIFICATE OF ANALYSIS Date: 9/14/01 <br /> Report# M253-09 <br /> Date Rec'd: 9/10/01 <br /> WHF Environmental Project: Boyett Petroleum-Quarterly Date Started.: 9/11/01 <br /> PO Box 427 Date Completed: 9/13/01 <br />' Oakdale CA 95361 PO# Date Sampled: 9/10/01 <br /> Time: <br /> Sample ID: MW-7 Sampler : R.Azevedo/R.Chrun <br />' <br /> Lab ID: M308844 <br /> Method RL Analyte Results Units <br /> 8260B 60 Benzene ND pg/L <br /> 60 Toluene ND <br /> 60 Ethyl Benzene ND <br /> 120 Total Xylenes ND <br /> 200 Methyl tert-butyl ether (MTBE) 20000 <br /> 8000 Ethanol ND <br />' 4000 tert-Butanol ND <br /> 200 di-Isopropyl ether (DIPS) ND <br /> 200 Ethyl tert-butyl ether (ETBE) ND <br /> 200 tert-Amyl methyl ether (TAME) ND <br />' 200 Ethylene dibromide (EDB) ND <br /> 100 1,2-Dichloroethane (1,2-DCA) ND <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% <br /> 1,2-Dichloroethane-d, 1000 1180 118.0 72-132 <br /> ' 2-Bromo-l-chloropropane 1000 885 88.5 71-134 <br /> 4-Bromofluorobenzene 1000 1130 113.0 74-132 <br /> ' Mario D'Onofrio ar Keller <br /> Chemist Certification # 1157 Laboratory Director <br />