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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209) 572-0916 <br /> Report# M253-09 CERTIFICATE OF ANALYSIS Date: 9/14/01 <br /> Date Recd: 9/10/01 <br /> WHF Environmental Project: Boyett Petroleum-Quarterly Date Started: 9/11/01 <br /> PO Box 427 Date Completed: 9/13/01 <br /> Oakdale CA 95361 PO# Date Sampled: 9/10/01 <br /> Time: <br />' Sample 1D: Trip Blank Sampler : R.Azevedo/R.Chrun <br /> Lab ID: M308347 <br /> Method RL AnalyteResults Units <br /> 8260B 0.3 Benzene_ ND pg/L <br /> 0.3 Toluene ND <br /> 0.3 Ethyl Benzene ND <br /> 0.6 Total Xylenes ND <br /> 1.0 Methyl tert-butyl ether (MTBE) ND <br /> 40 Ethanol ND <br /> 20 tert-Butanol ND <br /> 1.0 di-Isopropyl ether (RIPE) ND <br /> 1.0 Ethyl tert-butyl ether (ETBE) ND <br /> 1.0 tert-Amyl methyl ether (TAME) ND <br /> 1.0 Ethylene dibromide (EDB) ND <br /> 0.5 1,2-Dichloroethane (1,2-DCA) ND <br /> 1 <br /> i <br /> 1 <br /> 1 <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery OC 1•in-ir <br /> 1,2-Dichloroethane-d4 5.00 6.02 120.4 72-132 <br />' 2-Bromo-1-chloropropane 5.00 4.77 95.4 71-134 <br /> 4-Bromofluorobenzene 5.00 5.58 111.6 74-132 <br /> 1 Mario D'Onofrio Donna Keller < <br /> Chemist Certification # 1157 Laboratory Director <br />