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j SEQUOIA ANALYTICAL <br /> Chesapeake680 Redwood y, 063 <br /> (415) 364-9600 • FAX (415) 364-9233 <br /> Blaine Tech Services Inc Client Project 1D Shell, 420 Kettleman, Lodi Sampled Jan 25 1993 <br /> 985 Timothy Drive Sample Matrix Water Received Jan 27 1993 <br /> San Jose CA 95133 Analysis Method EPA 5030/8015/8020 Reported Feb 4 1993 <br /> Attention Glen Bennett First Sample # 3A40701 <br /> TOTAL PURGEABLE PETROLEUM HYDROCARBONS with BTEX DISTINCTION <br /> Reporting Sample Sample Sample Sample <br /> Analyte Limit I D I D II D I D <br /> ug/L 3A40701 3A40702 3A40703 3A40704 <br /> MW-1 MW-3 Dup Trip Blank <br /> Purgeable <br /> Hydrocarbons 50 N D N D N D N D <br /> Benzene 050 N D N D N D N D <br /> Toluene 050 N D N D N D N D <br /> Ethyl Benzene 0 50 N D N D N D N D <br /> Total Xylenes 050 N D N D N D N D <br /> Chromatogram Pattern <br /> Quality Control Data <br /> Report Limit <br /> Multiplication Factor 1 0 1 0 1 0 1 0 <br /> Date Analyzed 1/28/93 1/28/93 1/29/93 1/28/93 <br /> Instrument Identification GCHP-3 GCHP-3 GCHP-2 GCHP-3 i <br /> Surrogate Recovery, % 92 84 93 85 <br /> (OC Limits = 70-130%) <br /> Purgeable Hydrocarbons are quantitated against a fresh gasoline standard <br /> Analytes reported as N 0 were not detected above the stated reporting limit <br /> .SEQUOIA ANALYTICAL <br /> 'T I a/1 7 0 <br /> ria Lee <br /> roject Manager 3A40701 BlA < <br /> y r <br />