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7-1 <br /> THE OF` iNOCHLORINE PESTICIDES <br /> .' <br /> Twlj' Hig EPA METHOD 8081 <br /> LABORATORY CONTROL SPIKE <br /> ff <br /> LA 80 RAT0RIES , I NC . <br /> FRE SNO/MCOESTO/ISALA/BAKERS FIELD/SALINAS QUALITY CONTROL REPORT <br /> Analyzed By: Dara P. Vongkhampha Reviewed By: Joseph A. Ureno <br /> Date of Extraction: 02/24/2003 Date of Analysis: 02/25/2003 <br /> Twining Laboratories, Inc. Run ID Number: 022503 Sample Matrix: Soil <br /> Spike ID: WS 1823 COC Number: 70300847.1-14 <br /> Constituent Method Blank Laboratory Laboratory Laboratory Acceptable Laboratory Laboratory Relative <br /> Concentration Control Spike Control Spike Control Spike Percent Control Spike Control Spike Percenr'' <br /> (mg/kg) Concentration Recovery Duplicate Recovery Percent Duplicate Difference, <br /> Level (mg/kg) Recovery Range Recovery Percent (%) <br /> (mg/kg) (mg/kg) (%) (%} Recovery <br /> Low High (%) <br /> Lindane(Gamma-BHC) 0.000 0.042 0.040 0.035 52 1 130 95.2 83.3 13 <br /> Heptachlor 0.001 0.042 0.040 0.033 63 120 95.2 78.6 19 <br /> Dieldrin 0.000 0.042 0.039 0.035 58 120 92.9 83.3 11 <br /> Endrin 0.000 0.042 0.047 0.048 83 165 112 114 2.1 <br /> EXPLANATIONS <br /> ND Non-Detectable; the target analyte was not found above the detectable limit for reporting purposes(DLR). <br /> mg/kg milligrams per kilogram,parts per million(ppm)concentration units. <br /> Method Blank: The method blank is used to determine if method analytes or other interferences are present in the laboratory environment, <br /> the reagents or equpiment. <br /> Laboratory Control Spike: A laboratory control spike is generated by adding the target analyte(s)into a relatively inert matrix(sodium sulfatjor <br /> distilled water). The laboratory control sample is analyzed exactly like a sample,and its purpose is to determine <br /> the methodology is controlled and the laboratory is capable of making precise and accurate measurements. <br />