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i) 885 Jarvis Drive <br /> Sequoia • Morgan(Hill, 95037 <br /> 03 <br /> CA776-96M 9550370 <br /> IQF Analytical FAX(408)782-6308 <br /> Blaine Tech Services(Shell) Project: Shell Sampled: 4/18/00 <br /> 1680 Rogers Avenue Project Number: 305 S.Hutchins St.,Lodi Received: 4/20/00 <br /> San lose,CA 95112 Project Manager: Nick Sudano Reported: 5/11/00 10:10 <br /> Volatile Organic Compounds by EPA Method 80106/Quality Control <br /> Sequoia Analytical- Morgan Hill <br /> Date Spike Sample QC Reporting Limit Recov. RPD RPD <br /> lAnalyte Analyzed Level Result Result Units Recov.Limits % Limit % Notes* <br /> Blank(continued) OD18033-BLK2 <br /> Chlorobenzene 4/27/00 ND ug/1 0.500 <br /> Chloroethane ND 1.00 <br /> Chloroform ND 0.500 <br /> Chloromethane ND 1.00 <br /> Dibromochloromethane ND 0.500 <br /> 1,3-Dichlorobenzene ND 0.500 <br /> 1,4-Dichlorobenzene ND 0.500 <br /> 1,2-Dichlorobenzene ND 0.500 <br /> 1,1-Dichloroethane ND 0.500 <br /> 1,2-Dichloroethane ND 0.500 <br /> 1,1-Dichloroethene ND 0.500 <br /> cis-1,2-Dichloroethene ND 0.500 <br /> trans-1,2-Dichloroethene ND 0.500 <br /> 1,2-Dichloropropane ND 0.500 <br /> cis-1,3-Dichloropropene ND 0.500 <br /> trans-1,3-Dichloropropene ND 0.500 <br /> Methylene chloride ND 5.00 <br /> 1,1,2,2-Tetrachloroethane ND 0.500 <br /> Tetrachloroethene ND 0.500 <br /> 1,1,1-Trichloroethane ND 0.500 <br /> 1,1,2-Trichloroethane ND 0.500 <br /> 1,1,2-Trichlorotrifluoroethane ND 1.00 <br /> Trichloroethene ND 0.500 <br /> Trichlorofluoromethane ND 0.500 <br /> Vinyl chloride ND 1.00 <br /> 1,2-Dibromoethane ND 1.00 <br /> Surrogate: 4-Bromofluorobenzene /0.0 11.2 70-130 112 <br /> Blank OD1S033-BLK3 <br /> Bromodichloromethane 4/28/00 ND ug/1 0.500 <br /> Bromoforin ND 0.500 <br /> Bromomethane ND 1.00 <br /> Carbon tetrachloride ND 0.500 <br /> Chlorobenzene ND 0.500 <br /> Chloroethane ND 1.00 <br /> Chloroform ND 0.500 <br /> Chloromethane ND IF1.00 <br /> Dibromochloromethane ND 0.500 <br /> Sequoia Analytical-Morgan Hill *Refer to end of report for text of notes and definitions. <br /> Page 12 of 15 <br />