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A.., 110 2nd Avenue South 11D7 Pacheco CA 94553-5560 <br /> MCCampbell Analytical Inc. Telephone:925-798-1620 Fax:925-798-1622 <br /> F�Y" h ://www.rmcan7pbell.corn E-mail:rnain@mccampbelLcom <br /> ' Advanced GeoEnvironmental, Inc. Client Project ID: Van Buskirch Golf Date Sampled: 12/24/02 <br /> 837 Shaw Road Date Received: 12/27/02 <br /> ' Stockton,CA 95215 Client Contact: Bill Little Date Extracted: 12127102-12/30/02 <br /> Client P.O.: Date Analyzed: 12/27/02-12/30/02 <br /> MTBE and BTEX by GC/ MS* <br /> Extraction Method:SW5030B Analytical Method:SW82608 Work Order:0212434 <br /> ' Lab ID 0212434-005A 0212434-006A i 0212434-007A 0212434-008A <br /> i <br /> Client ID MW7/12-24-02 MW8/12-24-02 I` MW9/12-24-02 ; MW 10/12-24-02 Reporting Limit for <br /> Matrix ---- W — ---- _W I ------w --- --- W----- DF=1 <br /> DF — 1 1 10 —� 1 S W <br /> ' Compound Concentration ug/kg µg/L <br /> Benzene ND ND ND<5.0 ND NA 0.5 <br /> rF,thylbenzene ND ND ND<5.0 ND NA 0.5 <br /> Methyl-t-butyl ether(MTBE) ND ND 66 8.6 NA 0.5 <br /> Toluene ND<1,0 ND<1.0 ND<8.0 ND<1.0 NA 0.5 <br /> ' Xylenes ND ND ND<5.0 ND NA 0.5 <br /> Surrogate Recoveries(%) <br /> %SSI: 114 116 114 118 <br /> %SS2: 98.5 97.5 98.5 95.9 <br /> %SS3: 95.7 95.2 94.6 99.0 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soillsludge/solid samples in gg/kg, wipe samples in}tg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> h)lighter than water.immiscible sheen/product is present;i)liquid sample that contains greater than—2 vol.%sediment;j)sample diluted due to high <br /> ' organic content. <br /> 1 <br /> DHS Certification No, 1644Edward Hamilton,Lab Director <br />