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MINIMUM VERIFICATION LABORATORY ANALYSIS <br /> TANK TANK TPH-D TPH-D BTX do E CL 14C TOTAL EDB METALS PGH <br /> # CONTEMT'S 8015 8015 8020 8010 LEAD ICAP! 8270 <br /> 8260 8260 8260 8240 7420 8240 AES or 8080 <br /> 7421 AA <br /> 466 LEADED <br /> OAS X X X X <br /> UNL CI AS X X <br /> DIESEL X X <br /> KEROSENE X X <br /> UNK FUEL X X X X X <br /> OIL X X <br /> CTiLOR <br /> SOLVENTS X X <br /> NONCHLOR <br /> SOLVENTS X <br /> WASM <br /> USED OIL X X X X X <br /> All annlyses methods ate designated EPA,methods described in EPA SW 846,Thlyd Edition Those methods not found In <br /> SW 846, are specillcally noted below Refer to the "SWIkCH LUFT field Manual",Appendix A-20,Table 3-5 for detection <br /> limili of motor vehicle fuel't (gneollne and diesel) Refer to 1-2-3 "Regional Board Staff Recommendations for Initial <br /> Evaluation and Investigation of UST's" for the waste and motor oil detection limits <br /> I)etecllon 11mlii that remain below the MCL, STLC oP Allowable Umit of the conteminnnt In question will be nceepted, <br /> hoFvever inbornfor-y tholl trflllxe the most covtservative method. <br /> I A130RA MRY ANALYSES TERMINOLOGY: <br /> 11`110 Total Petroleum 1 lydrorarbon, Gaioline, OC/F lD (5030) 8015 moil or OCJMS 8260 <br /> 7 ri I D Total Petroleum hydrocarbon, Diesel, OCIFID (3550), 8015 mod or GCNS 8260 <br /> BTA etc E Bemene, Toluene, Xylene & Ethyl Benrene, GC/PID 8020 or GOMIS 8260 <br /> CL FIC Chlorinated Iydrocarbon, UC/HSD 8010, QCIMS 8240 <br /> Tout Lead Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> F09 Ethylene dibtomlde (I)TIS-AR 1803), GC/MS 8240 (DHS-Luft) <br /> OC T-ID Clat Chromalography, T-lame lonl7.atlon Detection <br /> ICA? or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000 MetnTq: Cudminvn, Chromium III and VI, Lend, avid Zinc. <br /> PCO Polychlorinated Diphenyls, ODMS 8270 or 8080 <br /> Method 1050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Mel hod 3550 Sonication sample preparation, extraction method <br /> Method 50301 Putge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Noles- To avoid false positive detection of bettaene, beniene-free solvents are to be used Fused capillary columns ate <br /> preferred to packed columns; a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons <br /> have been characterized and proper QA/AC Is followed <br /> ror Drinking water sources, LPA recommends that the 500 series for volatile organics be used in preference to the 600 series <br /> because the detection limits are lower the QA/QC Is better. <br /> Ell 23 048 (Rev I W190) page g <br />