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Method 5035 Sampling Page 3 of <br /> obtained on-line arly:�� <br /> ;a IIsIcY tali eta tat iaa <br /> The l' mer Handle <br /> 1. The blue plate should be in place on the Power Handle(flanges should be <br /> pointing to the round end of the handle). A 5g sample will be collected when <br /> the plate is in place. <br /> ?, Clip syringe into the Power Handle, <br /> 3. Using the Power Handle,push the syringe into the soil to collect 5g sample. <br /> 4. Unclip syringe from Power Iiandle and extrude 5.-sample into vial_ <br /> 5. Repeat process for each additional vial. <br /> 6. A single syringe can be used to collect sample aliquots for each of the three <br /> Mals. <br /> 7. Mark each sample container with your sample identification. Do not add any <br /> additional labels or tape to the pre.-tared vials. Store samples at 4"C.VOCs <br /> must be analysed within 14 days of collection. <br /> S. A fourth container needs to be submitted to the laboratory for percent total <br /> solids determination. Fill the container provided to capacity_ If extractable <br /> oro.anic analyses,i.e.,semi-volatiles, PNAs,or pesticides,'kBs will be <br /> Performed, rhe fourth container should be a 4-o/. glass jar. <br /> Note: Methanol is a flammable substance. If samples will be shipped to the <br /> laboratory via couriers such as UPS or Federal Express, DOT labeling requirements <br /> must he met. <br /> To meet DO I' labeling requirements,the following statement must be affixed to the <br /> package: <br /> "This package conforms to the conditions and limitations specified in 49CFR <br /> 173.4." <br /> The CFR reference is 49—Transportation, Part 173—Shippers,General <br /> Requirements for Shipments and Packaging, Section 173.4--Small Quantity <br /> Exceptions. In our opinion,the pertinent requirements of this reference are as <br /> follows: <br /> • -rhe maximum quantity of material per inner receptacle is limited to thirty <br /> (301 mL <br /> • Each inner receptacle is securely packed in an inside packaging with <br /> cushioning and absorbent material. The inside packaging cannot react <br /> chemically with the material and needs to be capable of absorbing the entire <br /> contents of the receptacle. (,Tote: the foartt cvrrrainer in whirl the Vials are <br /> placed greet these rcgr#ircmenis.) <br /> • The inside packaging is securely packed in a strong outside packaging. (Note: <br /> the cooler metas this regairenrew.) <br /> littp:/'www.firsteilv.coinl50')5sampling.litm 11/10/2009 <br />