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QC Sample Results C <br /> Client:Antea USA, Inc. TestAmerica Job ID: 720-56810-1 <br /> Project/Site: UPRR-Stockton <br /> Method: 8260B/CA_LUFTMS - 8260B/CA LUFT MS (Continued) <br /> Lab Sample ID: 720-56810-19 MS Client Sample ID: SO-2432-B-10D1.5-041614 <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 157833 Prep Batch: 157868 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> trans-1,2-Dichloroethene ND 0.0480 0.0455 mg/Kg 95 70-130 <br /> 1,2-Dichloropropane ND 0.0480 0.0484 mg/Kg 101 65-133 <br /> cis-1,3-Dichloropropene ND 0.0480 0.0537 mg/Kg 112 46-139 <br /> trans-l,3-Dichloropropene ND 0.0480 0.0600 mg/Kg 125 55-131 <br /> Ethylbenzene ND 0.0480 0.0452 mg/Kg 94 65-130 <br /> Hexachlorobutadiene ND 0.0480 0.0312 4 mg/Kg -1385 58-132 <br /> 2-Hexanone ND 0.240 0.231 mg/Kg 96 44-150 <br /> Isopropylbenzene ND 0.0480 0.0466 4 mg/Kg 97 65-130 <br /> 4-Isopropyltoluene ND 0.0480 0.0471 4 mg/Kg 98 69-134 <br /> Methylene Chloride 0.022 0.0480 0.0597 4 mg/Kg -4524 63-130 <br /> 8 <br /> 4-Methyl-2-pentanone(MIBK) ND 0.240 0.236 mg/Kg 98 51-140 <br /> Naphthalene ND 0.0480 0.0330 mg/Kg 69 45-146 <br /> N-Propylbenzene ND 0.0480 0.0499 4 mg/Kg -939 70-130 <br /> Styrene ND 0.0480 0.0497 mg/Kg 104 58-135 <br /> 1,1,1,2-Tetrachloroethane ND 0.0480 0.0590 mg/Kg 123 64-133 <br /> 1,1,2,2-Tetrachloroethane ND 0.0480 0.0545 mg/Kg 114 70-131 <br /> Tetrachloroethene ND 0.0480 0.0488 mg/Kg 102 67-130 <br /> Toluene ND 0.0480 0.0468 4 mg/Kg 98 70-130 <br /> 1,2,3-Trichlorobenzene ND 0.0480 0.0276 F1 mg/Kg 57 58-138 <br /> 1,2,4-Trichlorobenzene ND 0.0480 0.0322 mg/Kg 67 49-144 <br /> 1,1,1-Trichloroethane ND 0.0480 0.0530 mg/Kg 111 57-133 <br /> 1,1,2-Trichloroethane ND 0.0480 0.0508 mg/Kg 106 68-132 <br /> Trichloroethene ND 0.0480 0.0453 mg/Kg 94 66-130 <br /> Trichlorofluoromethane ND 0.0480 0.0439 4 mg/Kg -1939 61-130 <br /> 1,2,3-Trichloropropane ND 0.0480 0.0611 mg/Kg 127 62-150 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 0.0480 0.0405 mg/Kg 84 52.130 <br /> ne <br /> 1,2,4-Trimethylbenzene ND 0.0480 0.0538 4 mg/Kg 112 64-140 <br /> 1,3,5-Trimethylbenzene ND 0.0480 0.0545 4 mg/Kg -865 67-134 <br /> Vinyl acetate ND 0.0480 ND F1 mg/Kg 18 52-150 <br /> Vinyl chloride ND 0.0480 0.0447 mg/Kg 93 62-130 <br /> m-Xylene&p-Xylene ND 0.0960 0.0955 4 mg/Kg 100 70-130 <br /> o-Xylene ND 0.0480 0.0492 mg/Kg 102 68-130 <br /> 2,2-Dichloropropane ND 0.0480 0.0595 mg/Kg 124 63-130 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene 99 45-131 <br /> 1,2-Dichloroethane-d4(Surr) 119 60-140 <br /> Toluene-d8(Surr) 99 58-140 <br /> Lab Sample ID: 720-56810-19 MSD Client Sample ID: SO-2432-B-10D1.5-041614 <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 157833 Prep Batch: 157868 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Methyl tert-butyl ether ND 0.0467 0.0637 F1 mg/Kg 136 69-130 7 20 <br /> Acetone ND 0.234 0.193 4 mg/Kg 82 37.150 8 20 <br /> TestAmerica Pleasanton <br /> Page 178 of 241 4/29/2014 <br />