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QC Sample Results C <br /> Client:Antea USA, Inc. TestAmerica Job ID: 720-56810-1 <br /> Project/Site: UPRR-Stockton <br /> Method: 8260B/CA_LUFTMS - 8260B/CA LUFT MS (Continued) <br /> Lab Sample ID: 720-56810-19 MSD Client Sample ID: SO-2432-B-10D1.5-041614 <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 157833 Prep Batch: 157868 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,1,2,2-Tetrachloroethane ND 0.0467 0.0615 F1 mg/Kg 132 70-131 12 20 <br /> Tetrachloroethene ND 0.0467 0.0500 mg/Kg 107 67-130 2 20 <br /> Toluene ND 0.0467 0.0485 4 mg/Kg 104 70-130 3 20 <br /> 1,2,3-Trichlorobenzene ND 0.0467 0.0276 mg/Kg 59 58-138 0 20 <br /> 1,2,4-Trichlorobenzene ND 0.0467 0.0324 mg/Kg 69 49-144 0 20 <br /> 1,1,1-Trichloroethane ND 0.0467 0.0541 mg/Kg 116 57.133 2 20 <br /> 1,1,2-Trichloroethane ND 0.0467 0.0540 mg/Kg 116 68-132 6 20 <br /> Trichloroethene ND 0.0467 0.0467 mg/Kg 100 66-130 3 20 <br /> Trichlorofluoromethane ND 0.0467 0.0422 4 mg/Kg -1995 61-130 4 20 <br /> 1,2,3-Trichloropropane ND 0.0467 0.0706 F1 mg/Kg 151 62-150 14 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 0.0467 0.0410 mg/Kg 88 52-130 1 20 <br /> ne <br /> 1,2,4-Trimethylbenzene ND 0.0467 0.0566 4 mg/Kg 121 64-140 5 20 <br /> 1,3,5-Trimethylbenzene ND 0.0467 0.0579 4 mg/Kg -881 67-134 6 20 <br /> Vinyl acetate ND 0.0467 ND F1 F2 mg/Kg 10 52-150 54 20 <br /> Vinyl chloride ND 0.0467 0.0448 mg/Kg 96 62-130 0 20 <br /> m-Xylene&p-Xylene ND 0.0935 0.0974 4 mg/Kg 104 70-130 2 20 <br /> o-Xylene ND 0.0467 0.0505 mg/Kg 108 68-130 3 20 <br /> 2,2-Dichloropropane ND 0.0467 0.0586 mg/Kg 126 63-130 1 20 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene 97 45-131 <br /> 1,2-Dichloroethane-d4(Surr) 120 60-140 <br /> Toluene-d8(Surr) 102 58-140 <br /> Method: 8081A- Organochlorine Pesticides (GC) <br /> rLab Sample ID: MB 720-157769/1-A Client Sample ID: Method Blank <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 157880 Prep Batch: 157769 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Aldrin ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> Dieldrin ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> Endrin aldehyde ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> Endrin ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> Endrin ketone ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> Heptachlor ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> Heptachlor epoxide ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> 4,4'-DDT ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> 4,4'-DDE ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> 4,4'-DDD ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> Endosulfan I ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> Endosulfan 11 ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> alpha-BHC ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> beta-BHC ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> gamma-BHC(Lindane) ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> delta-BHC ND 0.0020 mg/Kg 04/21/14 14:21 04/22/14 20:17 1 <br /> TestAmerica Pleasanton <br /> Page 180 of 241 4/29/2014 <br />