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QC Sample Results C <br /> Client:Antea USA, Inc. TestAmerica Job ID: 720-56810-1 <br /> Project/Site: UPRR-Stockton <br /> Method: 60108 - Metals (ICP) (Continued) <br /> Lab Sample ID: LCSD 720-157814/3-A Client Sample ID: Lab Control Sample Dup <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 157888 Prep Batch: 157814 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Molybdenum 50.0 54.9 mg/Kg 110 80-120 14 20 <br /> Nickel 50.0 54.4 mg/Kg 109 80-120 13 20 <br /> Selenium 50.0 52.9 mg/Kg 106 80-120 13 20 <br /> Silver 25.0 25.6 mg/Kg 102 80-120 12 20 <br /> Thallium 50.0 55.1 mg/Kg 110 80-120 13 20 <br /> Vanadium 50.0 54.6 mg/Kg 109 80-120 13 20 <br /> Zinc 50.0 54.7 mg/Kg 109 80-120 13 20 <br /> Lab Sample ID: LCSSRM 720-157814/17-A Client Sample ID: Lab Control Sample <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 157888 Prep Batch: 157814 <br /> Spike LCSSRM LCSSRM %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Antimony 74.6 36.6 mg/Kg 49 11-101 <br /> Arsenic 45.5 44.5 mg/Kg 98 69-119 <br /> Barium 579 517 mg/Kg 89 61-117 <br /> Beryllium 155 151 mg/Kg 98 56-102 <br /> Cadmium 201 186 mg/Kg 93 67-118 <br /> Chromium 106 100 mg/Kg 95 67-121 <br /> Cobalt 247 234 mg/Kg 95 64-133 <br /> Copper 130 124 mg/Kg 95 68-126 <br /> Lead 302 281 mg/Kg 93 62-113 <br /> Molybdenum 165 158 mg/Kg 96 62-128 <br /> Nickel 305 286 mg/Kg 94 65-117 <br /> Selenium 133 130 mg/Kg 97 63-126 <br /> Silver 33.5 30.7 mg/Kg 91 51-130 <br /> Thallium 191 181 mg/Kg 95 64-124 <br /> Vanadium 214 205 mg/Kg 96 67-123 <br /> Zinc 388 369 mg/Kg 95 62-110 <br /> Lab Sample ID: 720-56810-41 MS Client Sample ID: SO-2432-B-28D3.5-041614 <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 157888 Prep Batch: 157814 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Antimony ND 46.7 11.3 F1 mg/Kg 23 75-125 <br /> Arsenic ND 46.7 43.1 mg/Kg 88 75-125 <br /> Barium 71 46.7 150 F1 mg/Kg 170 75-125 <br /> Beryllium ND 46.7 45.8 mg/Kg 97 75-125 <br /> Cadmium ND 46.7 44.7 mg/Kg 96 75-125 <br /> Chromium 39 46.7 85.7 mg/Kg 100 75-125 <br /> Cobalt 9.6 46.7 53.6 mg/Kg 94 75-125 <br /> Copper 25 46.7 70.2 mg/Kg 96 75-125 <br /> Lead 4.4 46.7 48.8 mg/Kg 95 75-125 <br /> Molybdenum ND 46.7 37.8 mg/Kg 80 75-125 <br /> Nickel 33 46.7 76.6 mg/Kg 93 75-125 <br /> Selenium ND 46.7 42.0 mg/Kg 88 75-125 <br /> Silver ND 23.4 21.8 mg/Kg 93 75-125 <br /> Thallium ND 46.7 42.7 mg/Kg 91 75-125 <br /> TestAmerica Pleasanton <br /> Page 197 of 241 4/29/2014 <br />