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r mepate Analysis 3 30 August 1997 <br /> Quarterly water samples for oxygenate compounds are to be taken from all monitoring wells <br /> at sites with 10 or fewer wells (supply wells and stuface water may be included in the <br /> monitoring program , as appropriate,by the Regio Board or Local Implementing Agency). <br /> At sites with more than ten monitoring wells,re qu is to change the sampling procedure must <br /> be approved by the Regional Board or Local Lnpler ienting,Agency. Soil samples should be <br /> analyzed beneath the primary leak source(s) (tank, ipeline, or dispenser) at regular depth <br /> intervals to the groundwater interface.If only MTB is found in the initial sampling/analysis, <br /> as confirmed by 8260,the Responsible Party may continue analysis by EPA Method 8020 for <br /> the oxygenate. Prior to requesting site closure a to cc nfirming round" for all oxygenate <br /> compounds must be completed. <br /> Laboratories must include all listed oxygenated s dards (TBA and Ethers) in their calibration <br /> standards and follow the QA/QC protocol detailec.in EPA Methods 8000 and 8020, or 8240-B <br /> or 8260, and the Code of Federal Regulations (CFR Title 40,parts 136.4 and 136.5). <br /> In addition to the compounds discussed above,we have found that both Tertiary amyl ethyl <br /> ether (TREE) and Isopropyl alcohol (IPA),WSPA, 997 data, also may be added to gasoline; <br /> and PRISTO (ethylene glycol monomethyl ether) is added to aviation fuel and,reportedly, <br /> some diesel fuels to prevent clog-ng of fuel lines t y microorganisms. Prist is registered as a <br /> pesticide with anti-microbial properties: CAS#OOC 109864. These compounds may be.added <br /> to the analysis list as more information becomes available. <br /> If you have questions,please call John Noo in Fresno at(209) 445-3550, <br /> Karen Cle tsen in Redding at(916) '-714-4852, ot me in Sacramento at (916) 255-3139. <br /> ON LEE BOGGS <br /> derground Tank <br /> rogram Manager <br />