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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572-0900 Fax(209)572-0916 <br /> port# S61)1311 Project: Pombo Ranch-Quarterly Date: 04/20/06 <br /> J. Kloberdattz&Associates Date Rec'd: 04/13/06 <br /> P.O. Box 576981 PON <br /> Modesto, CA 95357 <br /> CERTIFICATE OF ANALYSIS <br /> Sample ID: MW-4b Date Sampled: 04/13/06 <br /> Lab ID: S6D1311-04 Time: 10:43 <br /> Volatile Organic Chemistry of Hazardous Waste Sampler: Richard Chrun <br /> Method RL Analyte Result Units Notes Analyzed Batch# <br /> 8260B 0.3 Benzene ND ug/L 04/18/06 5001323 <br /> 0.3 Toluene ND ug/L <br /> 0.3 Ethylbenzene ND ug/L <br /> 0.6 Xylenes,total ND ug/L <br /> 0.5 Methyl tent-Butyl Ether(MTBE) 1.2 ug/L <br /> 40.0 Ethanol ND ug/L <br /> 5.0 cert-Butanol(TBA) ND ug/L <br /> 0.5 Di-isopropyl Ether(D1PE) ND ug/L <br /> 0.5 Ethyl tert-Butyl Ether(ETBE) ND ug/L <br /> 0.5 Tort-Amyl Methyl Ether(TAME) ND ug/L <br /> 1.0 Ethylene dibromide ND ug/L <br /> 0.5 1,2-Dichloroethane ND ug/L <br /> 5030/LUFT 0,05 Gasoline ND mg/L 04/14/06 5001319 <br /> aSurrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% Surrogate Notes <br /> a,a,a-Trifluorotoluene 0.0250 0.0229 92% 70-115 <br /> 1,2-Dichloroethane-d4 5.00 5.43 109% 72-131 <br /> 2-Bromo-l-Chloropropane 5.00 4.81 96% 71-134 <br /> 4-Bromofluorobenzcne 5,00 4.89 98% 74-132 <br /> Mario D'Onofrio Donna Keller <br /> Chemist Laboratory Director <br /> Certification #2585 <br />