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ANALYTI CAL <br /> LABORATORIES <br /> Paul Zumberge Certificate of Analysis <br /> Frontier Transportation, Inc. Report Issue Date: 02/28/2000 <br /> 3577 W. Philadelphia <br /> Chino, CA 91710 <br />' BSK Suhmission #: 2000020258 <br /> BSK Sample ID #: 23615 <br />' Project Ila: Project Desc: <br /> Submission Comments: <br /> Sample Type: Liquid Date Sampled: 02/04/2000 <br /> Sample Description. NNW-3 Time sampled: 1822 <br />' Sample Comments: Late Received: 02/07/2000 <br /> Oruanics Prep Analvsis <br /> Analvte Method Result Units POL Dilution DLR Date Date <br /> •UP]I as Diesel EPA 80I5(tv1) 33000 },g/L 50 10 500 02/15/2000 02/16/2000 <br /> TP11 as Gasoline EPA 8015(tvl) 3700 }tg/L 50 40 2000 02/14/2000 02/14/2000 <br />' TPH as hlowrOil EPA 8015(M) 33000 }tg/L 50 10 500 02/15/2000 02/16/2000 <br /> Beniene EPA 8020 150 lig/L 0.3 40 12 02/14/2000 02/14/2000 <br /> EYhylheniene EPA 8020 120 wg1L 0.3 40 12 02/14/2000 02/14/2000 <br /> lie Toluene EPA 8020 21 lag/1- 0.3 40 12 02/1412000 02/14/2000 <br /> Total Xytenes FPA 8020 280 Jig/l, 0.3 40 12 02/14/2000 02/14/2000 <br /> Di-isopropyl Ether EPA 8260 ND }Ig/L. 5.0 4 20 02/15/2000 02/15/2000 <br /> Ethyl t-Butyl Ell,cr EPA 8260 ND lig/L 5.0 4 20 02/15/2000 02/15/2000 <br /> Methyl-t-butyl Ether EPA 8260 90 }kg/I- 5-0 4 20 02/15/2000 02/15/2000 <br /> t-Aknv]Methvl Ekhrr EPA 8260 ND µg;L 5.0 4 20 02/15/2000 02/15/2000 <br /> IcIY-Bunvl Alcohol FPA 8261) ND µg11. 50 4 200 02/15/2000 02/15/2000 <br />' L-U1=T Comments <br /> "ITH as Diescl Lower boiling point hydrocarbons decreased relative to standard <br /> ]TH as Motor Oil Lower boiling point hydrocarbons decreased relative to standard <br />' tnt=_IL: millivntins/liter(ppm; POL: practical (mantitotion limit 11: analyzed outside of hold time <br /> ntt�lhP,: nlillil,ratnslkilol.rnli (1pm I) R: (It limit lilt rc°lxtrtin} f: prelirninaty result <br />' 1tUL: nucrograms/liter(ppb) : 11171,X IfIIk]tioll 5: suspect result <br /> 1tf'IK�: microkrams/kilogram(ppb; ND: node detected at DLR <br /> '!oRec: pereent recovered(surroRatesl <br />' 1.114 St;tnislaus Street Fresno,CA 93706-1623 Phone 559-497-258K, En CA 800-877-8310 Fax 559-485-693: <br />