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Entech Analytical Labs, Inc , Santa Clara, CA <br /> Lab Report No H3100301 Date 10/13/2003 Page 5 <br />' Project Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No NA Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-13 Lab Samp ID 36052-013 <br /> Descr/Location MW-13 Recd Date 10/03/2003 <br />' Sample Date 10/01/2003 Prep Date 10/06/2003 <br /> Sample Time 1930 Analysis Date 10/06/2003 <br /> Matrix Water QC Batch WMS210285 <br />' Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 03 1 PQL ND UG/L 1 <br /> 1,2-Dichlomethane 03 5 PQL ND UG/L 1 <br /> 1,2-Dibromoethane 05 5 PQL ND UG/L 1 <br />' SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-B ro mofluoro benzene 65-135 SMEA 942% 1 <br /> Toluene-d$ 77-150 SMEA 1012% 1 <br /> tDibromofluoromethane 57-156 SMSA 924% 7 <br /> 1 <br /> • <br /> I <br /> Approved by I Date 'J <br />