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Entech Analytical Labs, Inc , Santa Clara, CA <br /> Lab Report No H2101009 Date 10/21/2002 Page 11 <br /> Protect Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Protect No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW-7 Lab Samp ID 31582-001 <br /> Descr/Location MW-7 Recd Date 10/11/2002 <br /> Sample Date 10/07/2002 Prep Date 10/13/2002 <br /> Sample Time 1415 Analysis Date 10/13/2002 <br /> Matnx Water QC Batch WMS21748 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl4ert-butyl ether(MTBE) 03 5 PQL ND UG/L 1 <br />' Ethyl tert-butyl ether(ETBE) 05 5 PQL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 03 5 PQL ND UG/L 1 <br /> D;-isopropyl ether(DIPS) 05 5 PQL ND UG/L 1 <br /> tert-Butyl alcohol (TBA) 46 10 PQL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromofluorobenzene 65-135 SMEA 952% 1 <br /> Toluene-d8 77-150 SMEA 1011% 1 <br /> Dibromofluoromethane 57-156 SMEA 1000% 1 <br /> lie <br /> S <br /> 1 <br /> Approved by > Date <br />