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Itntech Analytical Labs, Inc , Santa Clara, CA <br /> Lab Report No H2101009 Date 10/21/2002 Page 1 <br /> Protect Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GCIMS Fuel <br /> Project No NA Method 8260FA <br /> I Prep Meth SW50306 <br /> I Field ID MW-1 Lab Samp ID 31582-013 <br /> 1 Descr/Location MWA Rec'd Date 10/11/2002 <br /> Sample Date 10/08/2002 Prep Date 10/14/2002 <br /> I Sample Time 1400 Analysis Date 10/14/2002 <br /> f Matrix Water QC Batch WMS21751 <br /> Basis Not Filtered Notes <br /> Analyte Det Lima Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 20 250 PQL 5800. UGIL 50 <br /> Ethyl tert-butyl ether(ETBE) 30 250 PQL ND UGIL 50 <br /> tert-Amyl methyl ether(TAME) 20 250 PQL ND UGIL 50 <br /> Di-isopropyl ether(DIPE) 30 250 PQL ND UGIL 50 <br /> tert-Butyl alcohol (TBA) 230 500 PQL ND UGIL 50 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromofluorobenzene 65-135 SMEA 98 2% 1 <br /> Toluene-d8 77-150 SMEA 1005% 1 <br /> I Dibromofluoromethane 57-156 SMEA 1016% 1 <br />! i <br /> E <br /> I <br /> I <br /> I <br /> t <br /> I <br /> Approved by 'y Date l� Z <br />