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Castle Analytical Laboratory,Atwater, CA <br /> Lab Report No H5031703 Date 03/30/2005 Page 1 <br /> roject Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GCIMS Fuel <br />' Project No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW-1 Lab Samp ID 7917-1 W <br /> Descr/Location MW-1 Recd Date 03!1812005 <br /> Sample Date 03/1812005 Prep Date 03/21/2005 <br />' Sample Time 1315 Analysis Date 03/21/2005 <br /> Matrix Water QC Batch VWMS-3215 <br /> Basis Not Filtered Notes DF <br />' Analyte Det Limit Rep Limit Note Result Units Pvc Oil <br /> Methyl4ert-butyl ether(MTBE) 289 500 -- MRL 340U UG/L. 1000 <br /> Ethyl tert-butyl ether(ETBE) 168 10 MRL NO UGIL 20 <br />' tert-Amyl methyl ether(TAME) 134 10 MRL 13 UG/L 20 <br /> Di-isopropyl ether(DIPS) 310 10 MRL NO UG/L 20 <br /> tert-Butyl alcohol (TBA) 176 400 MRL NO UG/L 20 <br />' SURROGATE AND INTERNAL STANDARD RECOVERIES 1 <br /> Toluene-d8 63.132 SLSA 956% <br /> 1,2-Dichlorcethane-d4 59-135 SLSA 959% 1 <br />' DF Reporting limits elevated due to matnx interferences <br /> lie <br />� <br /> 3 13 Ol I <br /> Approved by , Date �S <br /> I <br />