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' Castle Analytical Laboratory, Atwater, CA ` <br />' Lab Report No H5031703 Date 03/30/2005 Page 9 <br /> Project Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br />' Project No NA Method 8260FA <br /> Prep Meth SW5030B <br />' Field 10 MW-9 Lab Samp ID 7917-3W <br /> Descr/Location MW-9 Recd Date 03/18/2005 <br /> Sample Date 03/16/2005 Prep Date 03/21/2005 <br />' Sample Time 1155 Analysis Date 03/21/2005 <br /> Matnx Water QC Batch VWMS-3215 <br /> Basis Not Filtered Notes <br />' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 289 50 MRL 1400. UG/L 100 <br />' Ethyl tert-butyl ether(ETBE) 0 084 05 MRL 32 UG/L. 1 <br /> tert-Amyl methyl ether(TAME) 0 067 05 MRL 18 UG/L 1 <br /> Di-isopropyl ether(DIPE) 0155 05 MRL ND UGIL 1 <br />' tert-Butyl alcohol (TBA) 879 20 MRL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 63-132 SLSA 950% 1 <br />' 1,2-Dichloroethane-d4 59.135 SLSA 949% 1 <br />'� Y <br /> 1 <br /> 1 <br /> 1 <br /> 1 <br /> Approved Dy �C -� nate > 3 D D S <br />