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' Castle Analytical Laboratory,Atwater, CA <br /> Lab Report No H5031703 Date 03/30/2005 Page 5 <br /> rotect Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Protect No NA Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-16 Lab Samp ID 7917-7W <br /> Descr/Location MW-16 Recd Date 03/18/2005 <br /> Sample Date 03/16/2005 Prep Date 03/21/2005 <br /> Sample Time 1220 Analysis Date 03/21/2005 <br /> Matrix Water QC Batch VWMS-3215 <br /> Basis Not Filtered Notes <br />' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0 289 05 MRL ND UG/L ! <br />' Ethyl tert-butyl ether(ETBE) 0 084 05 MRL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0 067 05 MRL ND UG/L 1 <br /> Di-isopropyl ether(DIPE) 0155 05 MRL ND UG/L 1 <br />' tert-But l alcohol (TBA) 879 20 MRL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 63-132 SLSA 939% 1 <br />' 1,2-Dichloroethane-d4 59-135 SLSA 101% 1 <br /> lie r <br /> 1 <br /> 1 <br /> Approved by J8f/J P _ _ Uate 3 l 3oZO <br />