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Castle Analytical Laboratory, Atwater, CA <br /> Lab Repoit No H4100107 Date 10/11/2004 Page 1 <br /> Protect Name FRONTIER Analysis Volatile Organic Compounds by GCIMS Fuel <br /> Protect No 3RD QTR Method 8260FA <br /> Prep Meth SW5030B <br />' Field 1D MW-1 Lab Samp ID 7421-IW <br /> Descr/Location MW-1 Recd Date 10/01/2004 <br /> Sample Date 09/30/2004 Prep Date 10/0512004 <br />' Sample Time 1555 Analysts Date 10/05/2004 <br /> Matrix Water QC Batch VWMS-0054 <br /> Basis Not Filtered Notes DF <br /> FAnalyte Det Lima Rep Limit Note Result Units Pvc Dd <br /> t-butyl ether(MTBE) 578 100 MRL 8100 UG/L 200butyl ether(ETRE) 42 25 MRL ND UG/L 50 <br /> t tent-Amyl methyl ether(TAME) 335 25 MRL ND UG/L 50 <br /> Di-isopropyl ether(DIPE) 775 25 MRL ND UG/L 50 <br /> tent-Butyl alcohol (TBA) 4395 1000 MRL ND UG/L 50 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 63.132 SLSA 972% <br /> 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 927% 1 <br />' DF Reporting limits elevated due to matrix interferences <br /> 1 <br /> D <br /> 1 <br /> 1 <br /> 1 <br /> Approved by A 3 Date 0 E{ c? <br />