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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No H4010504 Date 01/1212004 Page 8 <br /> ect Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GCIMS Fuel <br /> 1:Proj <br /> Project No NA Method 8260FA <br /> Prep Meth SW50303 <br /> Field ID MW-3R Lab Samp ID 3491-3W <br /> Descr/Location MW-3R Rec'd Date 01/05/2004 <br /> Sample Date 12/30/2003 Prep Date 01/06/2004 <br />' Sample Time 1956 Analysis Date 01/06/2004 <br /> Matrix Water QC Batch VWMS-1064A <br /> Basis Not Filtered Notes DF <br />' Analyte Det Limit Rep Limit Note Result Units Pvc 01 <br /> Methyl-tert-butyl ether(MTBE) 578 100 MRL 600Q UG/L 200 <br /> Ethyl tert-butyl ether(ETBE) 168 10 MRL 14 UGIL 20 <br />' tert-Amyl methyl ether(TAME) 134 10 MRL 14 UGIL 20 <br /> Di-isopropyl ether(DIPS) 310 10 MRL ND UGIL 20 <br /> tert-Butyl alcohol (TBA) 176 400 MRL ND UGIL 20 <br />' 1,2-Dichloroethane 162 10 MRL ND UGIL 20 <br /> 1,2-Dibromoethane 184 10 MRL NO UGIL 20 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br />' Toluene-d8 76-129 SLSA 104% 1 <br /> 1,2-Dchloroethane-d4 53-141 SLSA 861% 1 <br /> DF Reporting limits elevated due to matrix interferences <br /> I <br /> 1 <br /> 1 <br /> Approved by Date t <br /> //2-1A el1 <br />