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` Castle Analytical Laboratory, Atwater, CA <br />` Lab Report No H4010504 Date 01/1212004 Page 10 <br /> f Protect Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Protect No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW-5 Lab Samp ID 6491-5W <br /> Descr/Location MW-5 Recd Date 01/05/2004 <br /> Sample Date 12/30/2003 Prep Date 01/06/2004 <br /> Sample Time 1517 Analysis Date 01/06/2004 <br /> Matrix Water QC Batch VWMS-1064A <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether (MTBE) 0 289 05 MRL ND UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) 0 084 05 MRL ND UG/L 1 <br /> tert-Amyl methyl ether (TAME) 0 067 05 MRL ND UG/L 1 <br /> Di-isopropyl ether(DIPS) 0155 05 MRL ND UG/L 1 <br /> tert-Butyl alcohol (TBA) 879 20 MRL ND UG/L 1 <br />' 1,2-Dichloroethane 0 081 05 MRL ND UG/L 1 <br /> 1,2-Dibromoethane 0 092 05 MRL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 70129 SLSA 115% 1 <br /> 1,2-Dichloroethane-d4 53.141 SLSA 103% 1 <br /> I • <br /> Approved by Date _ <br />