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' Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No H4032509 Date 04/05/2004 Page 18 <br /> Protect Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br />' Protect No NA Method 8260FA <br /> Prep Meth SW5030B <br /> t Field ID MW-9 Lab Samp ID 6796-9W <br /> Descr/Location MW-9 Recd Date 03/25/2004 <br /> Sample Date 03/24/2004 Prep Date 04/01/2004 <br />' Sample Time 1238 Analysis Date 04/01/2004 <br /> Matrix Water QC Batch VWMS-4014 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0 289 05 MRL 12 UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) 0 084 05 MRL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0 067 05 MRL ND UG/L 1 <br /> Di-isopropyl ether(DIPE) 0155 05 MRL ND UG/L 1 <br />' tert-Butyl alcohol (TBA) 879 20 MRL ND UG/L 1 <br /> 1,2-DEchlaroethane 0 081 05 MRL ND UG/L 1 <br /> 1,2-Dibromoethane 0 092 05 MRL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 76-129 SLSA 907% 1 <br /> 1,2-Dichloroethane-d4 53.141 SLSA 102% 1 <br /> 0 <br /> 1 <br /> t <br /> Approved by (V 1 Date `t <br /> 1 <br />