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nrr curl r-awr•urrmental Nerwol- WORK ORDER: 9711383 QUALITY CONTROL, REPORT PAGE QR-4 ANALYSIS: Metals] Scan' by ICP MATRIX: Water LABORATORY CONTROL SAMPLES ...................................................................... ....-----.........---•----•------•--•---•--•-.---••- SAMPLE TYPE: Spike-Method/Media blank LAB ID: IFW_LCS M INSTR RUN: ICP\971208035900/2/1 INSTRUMENT: TJA Enviro 36 PREPARED: BATCH ID: IFW120497-M . UNITS: mg/L ANALYZED: 12/08/97 DILUTION: 1.000000 METHOD: REF REPORTING SPIKE,, RECOVERY REC LIMITS (X) RPO ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RP0 (X) LIMIT (X) Ca Calcium 9.90 ND 0.2 10.0•.; 99.0 80 120 Cd Cadmium 0.0504 NO 0.005 0.0500;1 101 84 120 Co Cobalt 0.263 ND 0.005 0.250;1• 105 96 120 Cr Chromium 0.0998 ND 0.01 0.100;! 99.8 85 128 Cu Copper 0.124 NO 0.01 0.1251 99.2 86 123 Fe Iran 0.502 ND 0.1 0.500 r.100 84 133 K Potassium 9.94 NO 0.1 10.0 99.4 80 120 Mg Magnesium 10.2 ND 0.04 10.0 ! 102 80 120 Mn Manganese 0.261 NO 0.005 0.250;; 104 93 122 Mo Molybdenum 0.195 ND 0.01 0.200 97.5 89 117 Na Sodium 10.1 NO 0.5 10.0 101 80 120 Ni Nickel 0.255 NO 0.01 0.250.1 1 92 121 Pb Lead 0.516 NO 0.04 0.500,5 103 90 122 Sb Antimony 0.498 NO 0.02 0.500':' 99.6 82 113 V Vanadium 0.255 NO 0.005 0.250;1 1102 91 118 Zn Zinc 0.254 NO _0.01....... 0.250 ---- ..----90---. 102 121 ..... .......................... LABORATORY CONTROL DUPLICATES --------•-•------------------------------------------- ........ ---------------------------. ..••-.............. SAMPLE TYPE: Method Spike Sample Duplicate LAB ID: IFW LCR M INSTR RUN: ICP\971208035900/4/2 INSTRUMENT: TJA Enviro 36 PREPARED: - - BATCH ID: IFW120497-M UNITS: mg/L ANALYZED: 12/08/97 DILUTION: 1.000000 i METHOD: i #.� REF REPORTING ' SPIKE RECOVERY REC LIMITS (X) RPO ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) Ag Silver 0.0254 0.0254 0.005 0 10 Al Aluminum 1.07 1.01 0.1 5.77 10 . {. Ba Barium 1.05 1.00 0.01 4.88 10 Be Beryllium 0.0262 0.0254 0.002 3.10 10 Ca Calcium 10.3 9.90 0.2 3.96 15 Cd Cadmium 0.0491 0.0504 0.005 2.61 10 ' Co Cobalt 0.274 0.263 0.005 4.10 10 ' Cr Chromium 0.103 0.0998 0.01 3.16 10 Cu Copper 0.130 0.124 0.01 4.72 10 Fe Iron 0.520 0.502 0.1 3.52 10 K Potassium 10.3 9.94 0.1 3.56 10 Mg Magnesium 10.5 10.2 0.04 2.90 10 Mn Manganese 0.271 0.261 0.005 3.76 10 Mo Molybdenum 0.209 0.195 0.01 ` 6.93 10 Na Sodium 10.5 10.1 0.5 3.88 10 Ni Nickel 0.262 0.255 0.01 2.71 10 Pb Lead 0.533 0.516 0.04 3.24 10 Sb Antymony 0.518 0.498 0.02 3.94 10 V Vanadium 0.268 0.255 0.005 4.97 10 Zn Zinc 0.260 0.254 0.01 E 2.33 10 l • -----------*------ -- ------------------•-- ---...... ............-•-•----- ...-----••-••----•........... MATRIX SPIKE SAMPLES ............ .... ............................•....... .....-•--------•---------•------......... SAMPLE TYPE: Spike-Sample/Matrix LAB ID: MD11383-01E INSTR RUN: ICP\971208035900/17/15 INSTRUMENT: TJA Enviro 36 PREPARED: BATCH I0: IFW120497-M UNITS: mg/L ANALYZED: 12/08/97 DILUTION: 1.000000 METHOD. REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPO C, ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) Pb Lead 0.572 NO 0.04 0.5001` 114 67 131 .............•---.......-•-..... ....... ............. ..---... ......--•-................. �I