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Amcarl Environmental 1Vetivor-k <br /> WORK ORDER: 9710361 QUALITY CONTROL REPORT PAGE QR-4 <br /> ANALYSIS: Gasoline Oxygenates <br /> i <br /> MATRIX: Soil/Bulk. <br /> SAMPLE SURROGATES <br /> + L ................. <br /> ---•- <br /> SAMPLE TYPE: Sample-Client LAB ID: 97103617I06A INSTR RUN: GCMS12\971105000000/7/ <br /> INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS12S110597 <br /> UNITS: ug/kg ANALYZED: 11/05/0i DILUTION: 1.00 <br /> METHOD: REF REPORTING SPIKE D RECOVERY REC LIMITS (%) RPD <br /> I ANALYTE RESULT RESULT LIMIT VALUE (%) LOW HIGH RPD (%) LIMIT (%) <br /> 4 Bromofluorobenzene (surr) 95.6 100 100 T 95.6 70 130 <br /> { ..._....-•--•---••---...----•---•--•............................... ... - --•---------....- <br /> SAMPLE TYPE: Sample-Client LAB ID: 971036107A INSTR RUN: GCMS12\971105000000/8/ <br /> INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID; MS12S110597 <br /> UNITS: ug/kg ANALYZED: 11/06/97 DILUTION: 1.00 <br /> METHOD: <br /> REF REPORTING SPIKEryI RECOVERY REC LIMITS (%) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE'j (%) LOW HIGH RPD (%) LIMIT (%) <br /> { 1.2-DCE-d4 (surr) 92.4 100 100 'l 92.4 70 130 <br /> j Toluene d8 (surr) 96.7 100 100 y 96.7 70 130 <br /> 99.1 70 130 <br /> Bromofluorobenzene (surr) 99.1 100 100 J <br /> -- ----------------- •---......_...--•-- ---- -•-----.....__.......-----............. <br /> SAMPLE TYPE: Sample-Client LAB ID: 9710361208A INSTR RUN: GCMS12\971105000000/12/ <br /> INSTRUMENT: HP mass spec ___for Volatiles PREPARED: G BATCH ID: MS12S110597 <br /> UNITS: ug/kg ANALYZED: 11/06/97 DILUTION: 1.00 <br /> METHOD: REF REPORTING SPIKEI!( RECOVERY REC LIMITS (%) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE,; IM LOW HIGH RPD (%) LIMIT (%) <br /> 1,2-DCE-d4 (surr) 104 100 100 'k 104 70 130 <br /> Toluene-d8 (surr) 97.9 100 100 '1 97.9 70 130 <br /> Bromofluorobenzene (surr) 93.5 100 100 93.5 70 130 <br /> i SAMPLE TYPE: Sample-Client LAB ID: 9710361',09A INSTR RUN: GCMS12\971105000000/13/ <br /> i INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS12S110597 <br /> UNITS: ug/kg ANALYZED: 11/06/97 DILUTION: 1.00 <br /> METHOD: i <br /> REF REPORTING SPIKE',! RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUEI ;(%) LOW HIGH RPD (%) LIMIT (%) <br /> 1.2-DCE-d4 (surr) 114 100 100 `114 70 130 <br /> Toluene-d8 (surr) 96.0 100 100 ',i 96.0 70 130 <br /> Bromofluorobenzene (surr) 98.2 100 100 98.2 70 130 <br /> •.................................•-- .......... :. ----•--•---------------._..__......--•-_..._ <br /> SAMPLE TYPE: Sample-Client LAB ID: 9710361' 10A INSTR RUN: GCMS12\971105000000/15/ <br /> { INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS12S110597 <br /> UNITS: ug/kg ANALYZED: 11/06/97 DILUTION: 1.00 <br /> METHOD: <br /> j REF REPORTING SPIKE,, RECOVERY REC LIMITS (%) RPD <br /> ! ANALYTERESULT RESULT LIMIT VALUE; "(%) LOW HIGH RPD (%) LIMIT (1) <br /> 1.2-DCE-d4 (surr) 98.7 100 100 '„ 983 70 130 <br /> Toluene-d8 (surr) 95.8 100 10095.8 70 130 <br /> Bromofluorobenzene (surr) 95.3 100 100 95.3____-___70 130--•------_---- _ <br /> ......................................................... <br /> •-- <br /> ...................... ...... .............•---------••----•••------•-- ------ <br /> SAMPLE TYPE: Sample-Client LAB ID: 9710361-11A INSTR RUN: GCMS12\971105000000/14/ <br /> INSTRUMENT: HP mass spec for Volatiles PREPARED: BATCH ID: MS12S110597 <br /> UNITS: ug/kg ANALYZED: 11/06/97 DILUTION: 1.00 <br /> METHOD: <br /> REF REPORTING SPIKE; RECOVERY, REC LIMITS (%) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE'! (X) LOW HIGH RPD (%) LIMIT (%) <br /> 1.2-DCE-d4 (surr) 112 100 100 ',j 112 70 130 <br /> ,1 95.7 70 130 <br /> Bromofluorobenzene (surr) 95.0 100 100 <br /> Toluene-d8 (surr) 95.7 100 100 ' 95.0 70 130 <br /> LLL --------------------•---....-----....---•----•---..__...---.....----•----------.------.-..--.._..........----------..._.__. <br /> I � <br /> f <br />