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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mccaml2bell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Volpie Property Date Sampled: 07/08/98 <br /> 4005 North Wilson Way Date Received: 07/09/98 <br /> Stockton,CA 95205 Client Contact:Bill Little Date Extracted: 07/10-07/15/98 <br /> Client P.O: Date Analyzed: 07/10-07/15!98 <br /> Multi-Range(Gasoline,Diesel,Motor Oil)TPH as Diesel <br /> EPA methods modified 8015,and 3550 or 3510;California RNN'QCB(SF Bay Region)method GCFID(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(Gas)' TPH(Diesel)` TPH(N9otorOilf °/,Rcco%cry <br /> (C6-C12) (C10-C23) (>C18) Surrogate <br /> 91862 Ditch Water W ND 6500,g,d/b 62,000 104 <br /> 91864 TI-E S 19,000 10,000,b 7800 103 <br /> 91865 Tl-W S 4900 5900,b,d 81 --- <br /> 91866 TI-N S 15 3600,b,d 330 103 <br /> 91867 TI-Floor S ND ND ND 108 <br /> 91868 T3-1 S 1.1 88,d,g 390 96 <br /> 91869 T2 S 67 5.9,g 41 96 <br /> 91870 T4-1 S ND 2.4,b,g 6.0 107 <br /> 91871 T4-2 S ND ND ND 109 <br /> 91872 T4-3 S ND ND ND 107 <br /> 91873 SP-1-4 S 300 1900,d,g 15,000 969 <br /> Reporting Limit unless otherwise W 50 ug/L 50 ug/L 250 ug/L <br /> stated;ND means not detected above <br /> the reporting limit S 1.0 mg/kg 1.0 mg/kg 5.0 mg/kg <br /> *xNater samples are reported in ug/L,soil and sludge samples in mg/kg,wipes in ughvipe and all TCLP/SPLP extracts in mg/L <br /> cluttered chromatogram resulting in surrogate and sample peak coelution,or;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original extract. <br /> °oil-range compounds are not fully recovered by this GC methodology <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant;b)diesel range compounds are significant;no recognizable pattern;c) <br /> aged diesel?is significant);d)gasoline range compounds are significant;e)medium boiling point pattern that does not match diesel(?);f) <br /> one to a few isolated peaks present; g)oil range compounds are significant;h)lighter than water immiscible sheen is present; i)liquid <br /> sample that contains greater than—5 vol.%sediment. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />