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2.0 QUALITY ASSURANCE PLAN <br /> This section describes the field and analytical procedures to be followed throughout the investigation. <br /> 2.1 General Sample Collection and Handline Procedures <br /> Proper collection and handling are essential to ensure the quality of a sample. Each sample will be <br /> collected in a suitable container, preserved correctly for the intended analysis, and stored prior to <br /> analysis for no longer than the maximum allowable holding time. Details on the procedure for <br /> collection and handling of soil and ground water samples to be used on this project can be found in <br /> Section 1.0. <br /> 2.2 Sample Identification and Chain-of-Custody Procedures <br /> Sample identification and chain-of-custody procedures ensure sample integrity and document sample <br /> possession from the time of collection to its ultimate disposal. Each sample container submitted for <br /> analysis will have a label affixed to identify the job number, sampler, date and time of sample <br /> collection, and a sample number unique to that sample. This information, in addition to a <br /> description of the sample, field measurements made, sampling methodology, names of on-site <br /> personnel, and any other pertinent field observations will be recorded on the borehole log or in the <br /> field records. All samples will be analyzed by a California-certified laboratory. <br /> A chain-of-custody form will be used to record possession of the sample from time of collection to <br /> its arrival at the laboratory. When the samples are shipped, the person in custody of them will <br /> relinquish the samples by signing the chain-of-custody form and noting the time of shipment. The <br /> sample control officer will verify sample integrity and confirm that it was collected in the proper <br /> container, preserved correctly, and that there is an adequate volume for analysis. <br /> 2.3 Analytical Ouality Assurance <br /> In addition to routine calibration of the analytical instruments with standards and blanks, the analyst <br /> is required to run duplicates and spikes on 10 percent of the analyses to insure an added measure of <br /> precision and accuracy. Accuracy is also verified through the following: <br /> 1. EPA and State certification programs. <br /> 2. Participation in an interlaboratory or "round-robin" quality assurance program. <br /> 3. Verification of results with an alternative method. For example, calcium may be determined <br /> by atomic absorption, ion chromatography, or titrimetric methods. Volatile organics may be <br /> determined through either purge and trap or liquid-liquid extraction methods. <br />