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ENVIRON International Corp. Client Sample ID: GP-5 (6-71 ) GC/MS Volatiles Lot-Sample #...: GOG150480-009 Work Order #...: L38EGlAU Matrix- - - - - - - - - SOLID Date Sampled...: 07/14/10 Date Received..: 07/15/10 Prep Date......: 07/16/10 Analysis Date..: 07/16/10 Prep Batch #...: 0200274 Dilution Factor: 1.08 % Moisture.....: 24 Method. . ....... SW846 8260B REPORTING PARAMETER RESULT LIMIT UNITS MDL Dichlorodifluoromethane ND 7.1 ug/kg 1.3 (Freon 12) Trichlorofluoromethane ND 7.1 ug/kg 0.48 (Freon 11) Chloromethane ND 7.1 ug/kg 0.71 Vinyl chloride ND 7.1 ug/kg 0.51 Bromomethane ND 7.1 ug/kg 1.2 Chloroethane ND 7.1 ug/kg 0.64 1,1-Dichloroethene ND 7.1 ug/kg 0.37 Methylene chloride ND 14 ug/kg 1.2 trans-1,2-Dichloroethene ND 7.1 ug/kg 0.54 1,1-Dichloroethane ND 7.1 ug/kg 0.41 2,2-Dichloropropane ND 7.1 ug/kg 0.54 Bromochloromethane ND 7.1 ug/kg 1.3 Chloroform ND 7.1 ug/kg 0.37 1,1,1-Trichloroethane ND 7.1 ug/kg 0.51 Carbon tetrachloride ND 7.1 ug/kg 0.75 1,1-Dichloropropene ND 7.1 ug/kg 0.53 Benzene ND 7.1 ug/kg 0.37 1,2-Dichloroethane ND 7.1 ug/kg 1.0 Trichloroethene ND 7.1 ug/kg 0.85 1,2-Dichloropropane ND 7.1 ug/kg 0.85 Dibromomethane ND 7.1 ug/kg 0.83 Bromodichloromethane ND 7.1 ug/kg 0.75 cis-1,3-Dichloropropene ND 7.1 ug/kg 0.91 Toluene 3.1 J,B 7.1 ug/kg 0.87 trans-1,3-Dichloropropene ND 7.1 ug/kg 1.1 1,1,2-Trichloroethane ND 7.1 ug/kg 0.63 Tetrachloroethene ND 7.1 ug/kg 0.87 1,3-Dichloropropane ND 7.1 ug/kg 0.81 Dibromochloromethane ND 7.1 ug/kg 0.30 1,2-Dibromoethane (EDB) ND 14 ug/kg 0.38 Chlorobenzene ND 7.1 ug/kg 0.41 1,1,1,2-Tetrachloroethane ND 7.1 ug/kg 0.58 Ethylbenzene ND 7.1 ug/kg 0.48 m-Xylene & p-Xylene 4.7 J 7.1 ug/kg 1.2 o-Xylene 4.3 J 7.1 ug/kg 0.47 Styrene ND 7.1 ug/kg 0.44 (Continued on next page)