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1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> M C C a m p b e I l Analytical, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> � < <br /> "When Quality Counts" http://www.rmcanipbeU.com/E-mail:main@mccampbelf.com <br /> Quality Control Report <br /> Client: GeoRestoration,Inc. WorkOrder: 1407082 <br /> Date Prepared: 7/3/14 BatchID: 92364 <br /> Date Analyzed: 7/7/14 Extraction Method: SW3550C <br /> Instrument: HPLC4 Analytical Method: SW8310 <br /> Matrix: Soil Unit: mg/kg <br /> Project: #1163-3;Metalsa Sample ID: MB/LCS-92364 <br /> 1407082-008AMS/MSD <br /> QC Summary Report for SW8310 <br /> Analyte MB LCS RL SPK MB LCS LCS <br /> Result Result Val SS%REC %REC Limits <br /> Acenaphthene ND - 0.0050 - <br /> Acenaphthylene ND - 0.0050 - - - <br /> Anthracene ND - 0.0050 - - - <br /> Benzo(a)anthracene ND 0.0126 0.0050 0.015 - 84.2 70-130 <br /> Benzo(a)pyrene ND 0.0135 0.0050 0.015 90.2 70-130 <br /> Benzo(b)fluoranthene ND - 0.0050 - - - <br /> Benzo(g,h,i)perylene ND - 0.0050 - - - <br /> Benzo(k)fluoranthene ND - 0.0050 - - - <br /> Chrysene ND 0.0136 0.0050 0.015 90.9 70-130 <br /> Dibenzo(a,h)anthracene ND - 0.0050 - - - - <br /> Fluoranthene ND - 0.0050 - - - - <br /> Fluorene ND - 0.0050 - - - - <br /> Indeno(1,2,3)pyrene ND - 0.0050 - - - - <br /> 1-Methylnaphthalene ND 0.0155 0.0050 0.015 - 104 70-130 <br /> 2-Methylnaphthalene ND 0.0159 0.0050 0.015 - 106 70-130 <br /> Naphthalene ND - 0.0050 - - - - <br /> Phenanthrene ND 0.0139 0.0050 0.015 - 92.6 70-130 <br /> Pyrene ND 0.0129 0.0050 0.015 - 85.8 70-130 <br /> Surrogate Recovery <br /> Decafluorobiphenyl 0.856 - 1 86 - - <br /> 4,4-Dichlorobiphenyl 0.399 0.431 0.50 80 86 70-130 <br /> Analyte MS MSD SPK SPKRef MS MSD MS/MSD RPD RPD <br /> Result Result Val Val %REC %REC Limits Limit <br /> Benzo(a)anthracene 0.0120 0.0125 0.015 ND 80 83.4 70-130 4.09 30 <br /> Benzo(a)pyrene 0.0117 0.0122 0.015 ND 78.1 81.6 70-130 4.38 30 <br /> Chrysene 0.0130 0.0135 0.015 ND 86.9 90.1 70-130 3.64 30 <br /> 1-Methylnaphthalene 0.0160 0.0158 0.015 ND 107 105 70-130 1.49 30 <br /> 2-Methylnaphthalene 0.0161 0.0163 0.015 ND 107 109 70-130 1.23 30 <br /> Phenanthrene 0.0142 0.0147 0.015 ND 94.4 98.3 70-130 4.08 30 <br /> Pyrene 0.0128 0.0136 0.015 ND 85.5 90.3 70-130 5.45 30 <br /> Surrogate Recovery <br /> Decafluorobiphenyl 0.827 0.837 1 83 84 70-130 1.18 30 <br /> 4,4-Dichlorobiphenyl 0.445 0.447 0.50 89 89 70-130 0 30 <br /> CDPH ELAP 1644♦NELAP 4033ORELAP `' QA/QC Officer <br /> Page 53 of 65 <br />