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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9427-1 <br /> Matrix Spike/ Method: 8270C <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-22502 Preparation: 3550B <br /> MS Lab Sample ID: 720-9427-15 Analysis Batch: 720-22582 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22502 Lab File ID: c:\saturnws\epdata\data\2 <br /> Dilution: 1.0 Initial Weight/Volume: 30.39 g <br /> Date Analyzed: 06/11/2007 1402 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/08/2007 1525 Injection Volume: <br /> MSD Lab Sample ID: 720-9427-15 Analysis Batch: 720-22582 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22502 Lab File ID: c:\saturnws\epdata\data\20 <br /> Dilution: 1.0 Initial Weight/Volume: 30.47 g <br /> Date Analyzed: 06/11/2007 1431 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/08/2007 1525 Injection Volume: <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Naphthalene 51 57 21 - 133 10 35 <br /> Acenaphthene 53 56 40- 145 6 35 <br /> Acenaphthylene 56 60 33- 145 6 35 <br /> Fluorene 60 63 50- 121 3 35 <br /> Phenanthrene 55 58 10- 130 4 35 <br /> Anthracene 56 59 27- 133 5 35 <br /> Benzo[a]anthracene 57 60 33- 143 4 35 <br /> Chrysene 66 67 17- 168 2 35 <br /> Benzo[a]pyrene 65 66 17- 163 2 35 <br /> Benzo[b]fluoranthene 65 67 24- 159 4 35 <br /> Benzo[k]fluoranthene 69 72 11 - 162 5 35 <br /> Benzo[g,h,i]perylene 65 65 9-219 0 35 <br /> Indeno[1,2,3-cd]pyrene 61 64 9- 171 4 35 <br /> Fluoranthene 63 63 26- 137 2 35 <br /> Pyrene 62 65 52- 115 5 35 <br /> Dibenz(a,h)anthracene 60 63 52- 115 4 35 <br /> Surrogate MS% Rec MSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 56 60 30- 115 <br /> Terphenyl-d14 67 71 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> TestAmerica San Francisco Page 100 of 115 01/21/2008 <br />