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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9427-1 <br /> Matrix Spike/ Method: 8270C <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-22542 Preparation: 3550B <br /> MS Lab Sample ID: 720-9427-25 Analysis Batch: 720-22587 Instrument ID: Latest Chemstation <br /> Client Matrix: Solid Prep Batch: 720-22542 Lab File ID: 061107012.D <br /> Dilution: 1.0 Initial Weight/Volume: 30.27 g <br /> Date Analyzed: 06/11/2007 1929 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/11/2007 1204 Injection Volume: <br /> MSD Lab Sample ID: 720-9427-25 Analysis Batch: 720-22587 Instrument ID: Latest Chemstation <br /> Client Matrix: Solid Prep Batch: 720-22542 Lab File ID: 061107013.D <br /> Dilution: 1.0 Initial Weight/Volume: 30.37 g <br /> Date Analyzed: 06/11/2007 1956 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/11/2007 1204 Injection Volume: <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Naphthalene 61 57 21 - 133 7 35 <br /> Acenaphthene 64 60 40- 145 7 35 <br /> Acenaphthylene 68 65 33- 145 6 35 <br /> Fluorene 71 67 50- 121 6 35 <br /> Phenanthrene 70 65 10- 130 7 35 <br /> Anthracene 76 73 27- 133 4 35 <br /> Benzo[a]anthracene 77 76 33- 143 1 35 <br /> Chrysene 81 80 17- 168 2 35 <br /> Benzo[a]pyrene 77 74 17- 163 4 35 <br /> Benzo[b]fluoranthene 100 96 24- 159 5 35 <br /> Benzo[k]fluoranthene 78 75 11 - 162 4 35 <br /> Benzo[g,h,i]perylene 76 72 9-219 6 35 <br /> Indeno[1,2,3-cd]pyrene 82 79 9- 171 5 35 <br /> Fluoranthene 83 81 26- 137 3 35 <br /> Pyrene 80 80 52- 115 1 35 <br /> Dibenz(a,h)anthracene 85 80 52- 115 7 35 <br /> Surrogate MS% Rec MSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 68 57 30- 115 <br /> Terphenyl-d14 86 85 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> TestAmerica San Francisco Page 103 of 115 01/21/2008 <br />