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Analytical Data <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9470-1 <br /> Client Sample ID: TT-91-5 <br /> Lab Sample ID: 720-9470-21 Date Sampled: 06/11/2007 1718 <br /> Client Matrix: Solid Date Received: 06/12/2007 1240 <br /> 8270C Semivolatile Organic Compounds by GUMS(Selective Ion Monitoring) <br /> Method: 8270C Analysis Batch: 720-22732 Instrument ID: Sat 21<2 <br /> Preparation: 3550B Prep Batch: 720-22674 Lab File ID: c:\saturnws\epdata\data\200 <br /> Dilution: 10 Initial Weight/Volume: 30.30 g <br /> Date Analyzed: 06/15/2007 0511 Final Weight/Volume: 5 mL <br /> Date Prepared: 06/14/2007 0627 Injection Volume: <br /> Analyte DryWt Corrected: N Result(ug/Kg) Qualifier RL <br /> Naphthalene ND 250 <br /> Acenaphthene ND 250 <br /> Acenaphthylene ND 250 <br /> Fluorene ND 250 <br /> Phenanthrene 1200 250 <br /> Anthracene 340 250 <br /> Benzo[a]anthracene 380 250 <br /> Chrysene 1400 250 <br /> Benzo[a]pyrene ND 250 <br /> Benzo[b]fluoranthene ND 250 <br /> Benzo[k]fluoranthene ND 250 <br /> Benzo[g,h,i]perylene 520 250 <br /> Indeno[1,2,3-cd]pyrene ND 250 <br /> Fluoranthene 650 250 <br /> Pyrene 2500 250 <br /> Dibenz(a,h)anthracene ND 250 <br /> Surrogate %Rec Acceptance Limits <br /> 2-Fluorobiphenyl 77 30- 115 <br /> Terphenyl-d14 81 18- 137 <br /> STL San Francisco Page 23 of 55 06/19/2007 <br />