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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9415-1 <br /> Matrix Spike/ Method: 8270C <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-22459 Preparation: 3550B <br /> MS Lab Sample ID: 720-9415-7 Analysis Batch: 720-22505 Instrument ID: Latest Chemstation <br /> Client Matrix: Solid Prep Batch: 720-22459 Lab File ID: 060807007.D <br /> Dilution: 1.0 Initial Weight/Volume: 30.12 g <br /> Date Analyzed: 06/08/2007 1417 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/07/2007 1533 Injection Volume: <br /> MSD Lab Sample ID: 720-9415-7 Analysis Batch: 720-22505 Instrument ID: Latest Chemstation <br /> Client Matrix: Solid Prep Batch: 720-22459 Lab File ID: 060807008.D <br /> Dilution: 1.0 Initial Weight/Volume: 30.37 g <br /> Date Analyzed: 06/08/2007 1443 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/07/2007 1533 Injection Volume: <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Naphthalene 58 60 21 - 133 3 35 <br /> Acenaphthene 63 65 40- 145 1 35 <br /> Acenaphthylene 66 70 33- 145 4 35 <br /> Fluorene 71 71 50- 121 0 35 <br /> Phenanthrene 64 71 10- 130 9 35 <br /> Anthracene 77 83 27- 133 7 35 <br /> Benzo[a]anthracene 75 73 33- 143 2 35 <br /> Chrysene 79 76 17- 168 4 35 <br /> Benzo[a]pyrene 80 79 17- 163 1 35 <br /> Benzo[b]fluoranthene 90 91 24- 159 1 35 <br /> Benzo[k]fluoranthene 76 76 11 - 162 2 35 <br /> Benzo[g,h,i]perylene 76 74 9-219 4 35 <br /> Indeno[1,2,3-cd]pyrene 83 81 9- 171 4 35 <br /> Fluoranthene 79 85 26- 137 7 35 <br /> Pyrene 86 79 52- 115 9 35 <br /> Dibenz(a,h)anthracene 85 83 52- 115 2 35 <br /> Surrogate MS% Rec MSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 63 66 30- 115 <br /> Terphenyl-d14 89 86 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 53 of 64 06/14/2007 <br />