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CASTLE ANA�..,YTIG L � O_RATOR Pnon�: (209)364 z93a <br /> Environmental Testing Services 2333 Snuffle Drive,Atwater,CA 95301 }=ax; (209)384-1507 <br /> Certificate#2480 <br /> Client project Name:Premier Finishing Method:EPA 5030/82608 <br /> Shop Hazard Solutions,Inc, Lab Reference Number:3903100 instrument Ip;VARIAN M5 <br /> P.a.Box 798 Preparers: 03 29-99 <br /> Turlock,CA 95381 Sample Descripiinn;Water Analyzed: 03-29-19 <br /> Attn:Steve Meier Reported: 04-05-19 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE ID: VWMS-3299 <br /> BLANK Spiking Control °/°R <br /> Reporting Ike Limits <br /> Limit Result Level S p <br /> ug/L U01L a 1L %R <br /> CQMC'(JFlii]510 NO 75 iVA* 70-130% mm <br /> t-l3ut I Alcohol(t-8A) 0 50 ND 2 5 NA* 70-130°/° <br /> Mothyl t-butyl ether (I I'BE) 0 50 ND 2 5 NA" 70130°/° <br /> Diisopropyl ether{DIP3 } 13,160 <br /> 50 ND 2.5 NA- 70-130% <br /> Ethyl t But l ether(FTBE) 0.50 ND 2,5 NA* 70-130% <br /> t-Am I meth I ether{TAME 0,50 ND 2.5 NA* 70-130% <br /> 1,2 Dichlocoethane(1,2-D1;A) 0 50 ND 2.5 NAR 70-130% <br /> Eth lane dibromide(EDB) 0,50 ND NA* 70-130% <br /> 1,1-Dicnloroethene(1,1,bCF) 0.50 ND 2,5 NA* 70-130% <br /> Benzene 0.50 Nil 2.5 NA* 70 930% <br /> Trichloroethene(TOE) 0,60 D 2,5 NA* 70-130% <br /> Toluene 0.50 Nb 2.5 NA* 70-130% <br /> Chlnrobenzene <br /> Surra ate: 104°/° 10 NAR 70-130% <br /> Dibromofiuororriethane 1.0 10 70-•130% <br /> 1.0 107% NA` 70-130% <br /> 3,2-Dichloroetharie-d4 1.0 116% 10 NA* <br /> 1'o[uene as 1.0 96.3% 1q NAR 70130% <br /> 4-S�•oinofluorobe�tz�___,,.,e���._ <br /> CONTROL CONTROL %RPD <br /> Spiking SPIiGE bF1P Limits <br /> Level SPIKE <br /> u IL %R %R <br /> COMPOUNDS -� 0 81.7% 70-130% 4.33% <br /> 75 85.3/0 0.0% <br /> t-But I Alcohol(t-13A 7 5 96.8% 96.8% 70-130% <br /> Meth l t•-butyl ether (MTBE.) 80.0% 70-130% 29.4"/0 <br /> Diisoprop I ether(DIPE 2,5 3086/° ° To-130% 24.7% <br /> 2.5 111/0 86.41a 0 <br /> Ethyl t-Butyl ether(ETRE) 2,5 101% 86.0% 70-130% 15.85/° <br /> f-Am l meth I ether(TAME) 10G0/° 104% 70-130% 1.53% <br /> 1,2-Dichloraethane(1,2-DCA) 2.5 3.21°l0 a <br /> 2.5 114% 110°/0 70-130% <br /> Eth lene d'ibiomide{EDB) 2.5 95.6°/° 84,0b70-130°/0 12.44% <br /> 1,'9-DichloroethOne(1,1,DCE 95.6% 98 Q% 70-130% <br /> Benzene 2.5 <br /> 98.4/° 99,2/0 ° <br /> Trlohloroethene(TCE) 2.5 2.5 101% 100°l0 70-130% <br /> Toluene B3.6% 99,6% 70130% 17,5% <br /> Chlorobenzene 2.5 <br /> Surra ale: 10 -__ 109"/0 95.5%0 70-1:3D°/° _13.48% <br /> o <br /> Dlbromosluoromethane 1!3 125% � 109% 70-130°/a 14.0/0 <br /> 1.24pichloroethane-d4 :-124% - 101%-. <br /> Toluene-0 _� 1.0---- 103°l° 103%)° 70-130% 0.69% <br /> 4-B romofl uorobenzene <br /> 10 <br /> NA*See Conical 5piksl Central Spike Dup <br /> APPROVED T3Y: <br /> James G. P iflips/L oratory Director or <br /> Gari!. Cone/Lab refory Manager <br />