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MII,C-11796B <br /> arrangement. Apply a 100-gram load on top remove a 1-inch strip of the coating along <br /> �of each of the three assembled panel sets, one of the long edges of the panel, after cut- <br /> And place them in a horizontal position for ting the film parallel to the edge of the panel, ; <br /> 24 hours in a forced-draft oven maintained and at a right angle to the surface of the <br /> .at 180 ± 2° F. At the end of the heating panel. A straight line shall then be drawn or <br /> period remove the panels from the oven and scratched on the panel, parallel to the cut <br /> decoat using naphtha. Inspect the panels for edge of the film, and 1/8 inch away from it. <br /> evidence of stain, discoloration, or corrosion, The panel shall then be suspended vertically, <br /> disregarding the outer 1/8 inch edges of .the with the exposed area downward, for 4 hours <br /> panels. in a gravity convection oven maintained at <br /> 150 ± 2° F. for Class 1 or 1A compound; <br /> 4.6.9 Low temperature adhesion. A test 1450 ± 2° F. for Class 2 compound; or <br /> 130° ± 2° F. for Class 3 compound. The <br /> panel shall be cleaned and polished (see panel shall be .removed from the oven and <br /> 4.6.8.1), and coated (see 4.6.8.1.2) with a allowed to cool to room temperature. The <br /> film of 1.5 --±:,0.2 mils. After standing for <br /> approximately 16 hours, the panel shall be position of ;the cut edge of the coating, rela- <br /> tive to the reference line drawn or scratched <br /> cooled to —40 ±3° F. and maintained at <br /> this temperature for a minimum of one on the panel, shall then be observed. The <br /> compound shall then be considered to fail <br /> hour. While at this temperature 4 parallel the flow point requirements if any movement <br /> scratches, approximately 1/8 of an inch apart <br /> and 1 inch long, shall be made on the film in of the coating toward the reference line has <br /> one direction, and 4 other similarr scratches occurred as a result of heating at the ap- <br /> made at right angles to them, so as ,to form plicable specified temperature. <br /> a checkered pattern on the coating. A 4- <br /> bladed instrument, shown in figure 3, is 4.6.11 Removability. <br /> recommended for making the scratches. The <br /> tool shall be kept at ambient room tempera- 4.6.11.1 Apparatus. A satisfactory appara- <br /> tuTe. In making the scratches the tool shall tus for determining removability property <br /> be held in such a position that the cutting of the compound is illustrated in figure 4. <br /> edges make a 45° angle with the surface of The essential component of the apparatus is <br /> ` the film, and shall be drawn at a rate of the rubbing device, which is shown in detail <br /> approximately 1 inch per second through the in figure 5. The device consists of a glass <br /> film. The compound shall be considered un- tube having an open bulb at one end, and a <br /> satisfactory in adhesive qualities if there is felt plug at the other end. A felt plug, which <br /> any flaking of the film within the areas protrudes approximately 1/8-inch from the <br /> bounded by the scratches. Flaking shall be end of the tube, serves as the rubbing mem- <br /> -defined as chipping of the film for a distance ber. The rubbing tool is supported vertically <br /> greater than 1/32 of an inch on either side of and is drawn back and forth across the sur- <br /> the scratch marks. If a retest is authorized face of the coated panel. A continuous flow <br /> by the Government in case of failure, new of dry-cleaning solvent, conforming to Speci- <br /> blades shall be used in the cutting tool to fication P-S-661, is maintained through the <br /> eliminate wear of the blade edges as a factor tube, the felt plug, and over the test panel <br /> in the outcome of the retest. as the rubbing action Makes place. The rub- <br /> bing tool is free to exert its own weight, plus <br /> 4.6.10 Flow point. A test panel shall be that of the solvent it contains, upon the <br /> cleaned and polished (see 4.6.8.1),and coated surface of the panel. A constant head of <br /> with a film of 50 to 55 mils (see 4.6.8.4). solvent is maintained during the entire test <br /> Using a stiff spatula, knife, or razor blade by means of the assembly shown in figure 4. <br /> 9 <br />