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12/02/2012 21:41 20 339 G- SANBORN PAGE 09/09 <br /> I 53d Willow Pim Road.Pimsburg,CA 94565.1701 <br /> M c C a m be I I Anas l fical, Inc, Tvil free Telephtme:(877)232-9262 1 Fns:(925)252-9269 <br /> r <br /> When Q41,711 �rxrnly" lrtpJh3%vw.mccampbell.com'E-mail: nain(_B,mccampl;ell,rcrn <br /> QC SUMMARY REPORT FOR SW6020 <br /> W,0.Sample Matrix: Scil QC Matrix; Soil BatchlD: 71924 WorkOrder; 1210955 <br /> EPA Method: S1N6020 Extraction: SW30608 Spiked Sample ID: 121OS22.031A <br /> Analyte Sample_ Spiked NIS MSD MS-MSD LCS Acceptance Criteria(°h) <br /> mg/Kg mg1Kg % Rec. % Rec. %RPD %Rec, MS!MSD RPD LCS <br /> Antimony 0.54 50 104 106 1.51 109 75-125 1 20 75-125 <br /> arsenic 63 50 105 109 3 38 1.17 75- 125 20 75.125 <br /> HariLlln 110 500 ill 11.4 a 2.02 105 15- 125 20 75•I25 <br /> Beryllium 0,72 50 89.4 90.6 1.38 115 75-125 20 75- 125 <br /> Cadmium ND 50 104 105 1.52 Ill 75-125 20 75-125 <br /> Chromium 67 50 l U7 l l5 3.26 113 75-125 20 75- 125 <br /> Cohan _-_ - is ^-- 50 99.7 l02 1.89 107 75-125 20 75-125 <br /> Copper 36 50 r 106 ?11 I 3.04 1:'7 75- l25 20 75-125 <br /> Lead 9.4 50 106 107 4 0.672 120 75-125 20 75-125 <br /> Mercury 0.082 1 25 99.5 98.3 1,14 123 75- 125 20 75-125 <br /> M01yhdcnum :.4 50 106 109 2,49 l lu 75-125 20 T 75-125 <br /> Nickel 31 50 111 120 3.45 115 75- 125 20 1 75,125 <br /> Selenium ND 50 103 1.07 4.212 11.7 75-12$ 20 7$-125 <br /> Silver ND 50 103 104 0.714 Ili 75. 125 20 75- 125 <br /> Thallium NTS 50 97.9 1 97.5 0,408 118 75- 125 20 75-125 <br /> Vanadium _ 67 50 105 1 112 3.05 115 75- 125 20 75-1.25 <br /> Zinc 80 500 105 108 2.44 117 75. 125 20 1 75.125 <br /> %SS. 10 500 114 110 ).01. 112 70-130 20 70-130 <br /> All target compound;in the Method?lank of his extraction batch wercNM less than tlyc method Rl.,with the followingcxoepdoDS: <br /> NONE <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> I 210855-00 1 A I Gi25J12 18/25/12 10/29/12 5.41 PM 1210955-001 A 10/25/12 10125!12 10/29/12 8:15 PM <br /> 1210855.00;A 10/25/12 10/25112 10<9/12 9 33 Ply] . 1210855-001 A 10,x25/12 10!25112 1013 1/12 91-37 PM <br /> M$G Matrix Spike;MSD=Matrix 5plke Dup tile: CS=Laboratory t.ontrel 5arple'LCSD=LaboratGry Control Sample Duplicate!RPD=Relative Percent Devlation. <br /> %Recavery=100"(MS-Sample)I(Amount Spikeil);RPD=106-(MS• MSG)I((MS+MSD)12), <br /> MS I-VSD spike recoverles and I or%RPD may fetl'loutslde of laboratory acceptance criteria due to one or more of the following reasons;a)the sample is inhomogenous AND contains <br /> Significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix Interferes*Ih the spike recovery, <br /> MA=not applicable to this mathod. <br /> NR=analyte concentration in Sam 19 exceeds a ikk amount for Soil matrix or exceeds 2x s ke amOUnt for water matrix orsarriple diluted due to hiph matrix or anal to content. <br /> DHS FLAP Certification 1644 � QA/QC Officer <br />