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�� McCamabell Analytical Inc 1534 Willow Pass Road,Pittsburg,CA 9d565-1701 <br /> Web:www.mccampbell.cam &mail:main@mccampbell.com <br /> "When Oualiry Counts" Tele hone:877-252-9262 Fax:925-252-9269 <br /> ' QC SUMMARY REPORT FOR E350.1 <br /> W.O.Sample Matrix: Soil QC Matrix: Soil BatchlD: 44103 WorkOrder 0906751 <br /> EPA Method E350.1 Extraction SM4500-Norg B Spiked Sample ID: 0906751-001A <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg mg/Kg -/.Rec. %Rec. %RPD %Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> Total Ammonia as N NO 40 101 100 1 0.185 99.2 1 98.7 1 0.466 80- 120 1 20 90- 110 1 20 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 44103 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0906751-001A 06/02/09 06/24/09 07/01/09 11:10 AM <br /> MS= iii:::; ;::1 Spike;MSD=MaMx Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laborerory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> ' %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100 (MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> ' N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte centent. <br /> DHS ELAP Certification 1644 <br /> QA/QC Officer <br />