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' .(�� McCamobell Analytical Inc 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> Web:www.mccampbell.com E-mail:mainQmccampbell.com <br /> "When Oualiw Counts" Tele hone:877-252-9262 Fax:925-252-9269 <br /> ' QC SUMMARY REPORT FOR E365.3 <br /> W.O.Sample Matrix: Soil OC Matrix: Soil BatchlD: 44757 WorkOrder: 0906751 <br /> EPA Method E365.3 Extraction E365.3 Spiked Sample ID: 0906804-001A <br /> ' Analyte Sample VIS MSD MS-MSD LCS I LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg I mg/Kg I%Rec. %Rec. %RPD %Rec. %Rec. %RPD I MS/MSD RPD LCS/LCSD RPD <br /> ' Total Phosphorous as P270 40 NR NR NR 97.3 98 0.700 80- 120 20 90- 110 1 20 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 44757 SUMMARY <br /> ' Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0906751-001A 06/02/09 07/23/09 07/30/09 2:23 PM <br /> ' MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> ' %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=too-(MS- MSD)/((MS+MSD)12). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> ' N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> ' DHS ELAP Certification 1644 QA/QC Officer <br />