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Inc.McCampbell Analytical, IAL 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> ' Web:welepho e:877-252- limak:main@52-mail;"When Quality Counts" Telephone: 262 Fl;main mcca269 <br /> QC SUMMARY REPORT FOR CA Test 417/422 <br /> ' W.O.Sample Matrix: Soil QC Matnx: Soil BatchlD: 44470 WorkOrder: 0906804 <br /> EPA Method CA Test 4171422 Extraction CA Test 4171422 Spiked Sample ID: N/A <br /> ' Analyte Sample Spiked I MS I MSD MS-MSD LCS I LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg mgi %Rec. %Rec. %RPD %Rec. I%Rec.I %RPD MS/MSD I RPD I LCS/LCSDRPD <br /> ortho-Phosphate N/A 30 1 N/A N/A N/A 91.8 91.4 0.429 N/A N/A 80- 120 20 <br /> ./.Ss: N/A 3 1 N/A N/A N/A 91 1 91 1 0 N/A N/A 80- 120 20 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> ' BATCH 44470 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0906804-OOIA 06/25/09 11:55 AM 07/13/09 07/14/09 9:56 PM I 0906804-002A 06/25/09 10:00 AM 07/13/09 07/14/09 10:37 PM <br /> 1 <br /> MS=Mai Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> 11 Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not applicable to this method. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> ue <br /> DHS ELAP Certification 1644 QA/QC Officer <br />