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man <br /> Report Number: 69398 <br /> QC Report : Matrix Spike/ Matrix Spike Duplicate Date : 07/30/2009 <br /> Project Name : Sara Lee-Lincoln <br /> Project Number: 62403335 <br /> Duplicate Spiked <br /> Duplicate Spiked Spiked Sample Relative <br /> Spike Spiked Spiked Sample Sample Relative Percent Percent <br /> Spiked Sample Spike Dup. Sample Sample Analysis Date Percent Percent Percent Recov. Diff. <br /> Parameter Sample Value Level Level Value Value Units Method Analyzed Recov. Recov. Diff. Limit Limit <br /> 1,2-Dichloroethane 69381-01 <0.50 40.7 40.7 41.0 40.7 ug/L EPA 8260B 7/25/09 101 100 0.820 70-130 25 <br /> Benzene 69381-01 140 40.5 40.5 162 167 ug/L EPA 8260B 7/25/09 47.1 59.0 22.3 70-130 25 <br /> Methyl-t-butyl ether 69381-01 1.9 40.6 40.6 38.8 37.9 ug/L EPA 8260B 7/25/09 90.8 88.6 2.56 70-130 25 <br /> Tert-Butanol 69381-01 <5.0 201 201 201 205 ug/L EPA 8260B 7/25/09 100 102 1.83 70-130 25 <br /> Toluene 69381-01 47 40.0 40.0 79.5 81.4 ug/L EPA 82606 7/25/09 81.8 86.5 5.58 70-130 25 <br /> 1,2-Dichloroethane 69398-03 <0.50 40.8 40.8 37.0 37.4 ug/L EPA 8260B 7/25/09 90.8 91.9 1.18 70-130 25 <br /> Benzene 69398-03 <0.50 40.6 40.6 37.3 37.4 ug/L EPA 82606 7/25/09 91.9 92.2 0.369 70-130 25 <br /> Methyl-t-butyl ether 69398-03 <0.50 40.7 40.7 35.8 36.4 ug/L EPA 8260B 7/25/09 88.0 89.5 1.66 70-130 25 <br /> Tert-Butanol 69398-03 <5.0 201 201 190 195 ug/L EPA 8260B 7/25/09 94.2 96.6 2.51 70-130 25 <br /> Toluene 69398-03 <0.50 40.1 40.1 39.2 39.2 ug/L EPA 8260B 7/25/09 97.7 97.6 0.0449 70-130 25 <br /> 1,2-Dichloroethane 69398-08 1.2 40.8 40.8 39.1 38.4 ug/L EPA 8260B 7/27/09 93.1 91.4 1.85 70-130 25 <br /> Benzene 69398-08 180 40.6 40.6 220 217 ug/L EPA 8260B 7/27/09 92.0 86.3 6.47 70-130 25 <br /> Methyl-t-butyl ether 69398-08 2.2 40.7 40.7 38.3 38.2 ug/L EPA 8260B 7/27/09 88.6 88.4 0.302 70-130 25 <br /> Tert-Butanol 69398-08 10 201 201 202 203 ug/L EPA 8260B 7/27/09 95.4 95.6 0.229 70-130 25 <br /> Toluene 69398-08 2.7 40.1 40.1 42.6 42.3 ug/L EPA 8260B 7/27/09 99.4 98.7 0.715 70-130 25 <br /> 1,2-Dichloroethane 69405-11 <0.50 40.8 40.8 37.8 37.3 ug/L EPA 8260B 7/27/09 92.8 91.6 1.29 70-130 25 <br /> Benzene 69405-11 <0.50 40.6 40.6 38.2 37.2 ug/L EPA 8260B 7/27/09 94.1 91.6 2.68 70-130 25 <br /> Methyl-t-butyl ether 69405-11 <0.50 40.7 40.7 35.8 35.3 ug/L EPA 82608 7/27/09 88.0 86.6 1.50 70-130 25 <br /> Tert-Butanol 69405-11 <5.0 201 201 190 190 ug/L EPA 8260B 7/27/09 94.2 94.1 0.0328 70-130 25 <br /> KIFF ANALYTICAL, LLC <br /> 2795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800 <br />