Laserfiche WebLink
®� McCampbell Analytical. Inc. 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> 1 Web:www.mecampbell.com Email:main@mccampbell.00m <br /> "When Oualiw Counts" 7 Tele hone:877-252-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR E350.1 <br /> W.O.Sample Matrix: Water QC Matrix: Water BatchlD: 44665 WorkOrder 0907603 <br /> EPA Method E350.1 Extraction E350.1 Spiked Sample ID: 0907514-014D <br /> 1 Analyte Sample Spiked I MS I MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/L mg/L %Rec. %Rec. %RPD %Rec. %Rec. %RPD I MS/MSD RPD LCS/LCSD RPD <br /> 1 Total Ammonia as N 0.58 4 1 98 1 98 1 0 108 104 3.96 80- 120 1 20 90- 110 20 <br /> All target compounds in the Method Blank of this extraction batch were NO less than the method RL with the following exceptions: <br /> NONE <br /> 1 BATCH 44665 SUMMARY <br /> 1 Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0907603-OOIE 07/22/09 2:20 PM 07/23/09 07/23/09 '' 12 AM 0907603-002E 07/22/09 1:25 PM 07/23/09 07/23/09 11:56 AM <br /> 0907603-003E 07/22/09 12:10 PM 07/23/09 07/23/09 12:00 PM 0907603-004E 07/22/09 10:20 AM 07/23/09 07/23/09 12:03 PM <br /> 1 <br /> i <br /> 1 <br /> i <br /> 1 <br /> 1 <br /> 1 MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate',RPD=Relative Percent Deviation. <br /> 1 %Recovery=100`(MS-Sample)/(Amount Spiked);RPD=100•(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount Spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> 1 N/A=not applicable to this method. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS FLAP Certification 1644 J2— QA/QC Officer <br /> 1 <br />