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Alpha Analytical, Inc. <br /> 255 Glendale Ave • Suite 21 • Sparks, Nevada 89431-5778 <br /> (775) 355-1044 •(775)355-0406 FAX• I-800-283-1183 <br /> Date <br /> 14-Nov-03 QC Summary RepWork Order <br /> ort 03110544 <br /> Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID D 1HPCHEMIMS091DATA1031106103110606 D Batch 1D MS9W1106A Analysis Date 11/06/2003 10 53 <br /> Sample ID MBLK MS9W1106A Units pg/L Run ID GCIMSD_9_031106A Prep Date 11/06/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual <br /> Tertiary Butyl Alcohol (TSA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 05 <br /> Di-isopropyl Ether(D1PE) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETRE) ND 1 <br /> Benzene ND 0 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 0 5 <br /> Ethylbenzene ND 0 5 <br /> m,p-Xylene ND 0 5 <br /> o-Xylene ND 0 5 <br /> Surr 1 2-Dichloroethane-d4 109 10 109 72 126 <br /> Surr Toluene-d8 971 10 97 71 128 <br /> Surr 4-Bromofluorobenzene 953 10 95 76 121 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> File 1D D IHPCHEM%MS091DATA1031106103110604 D Batch ID NIS9W1106A Analysis Date 91/06/2003 10 02 <br /> Sample ID LCS MS9W1106A Units lig/L Run ID GC/MSD_9_031106A Prep Date 11/06/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimd Highl-imit RPD Ref Val %RPD Qual <br /> Benzene 931 0 5 10 93 83 119 <br /> Toluene 8 76 0 5 10 88 80 120 <br /> Ethylbenzene 932 0 5 10 93 80 120 <br /> m,p-Xylene 187 05 20 93 77 125 <br /> eo-Xylene 932 0 5 10 93 77 124 <br /> urr 1 2-Dichloroethane-d4 107 10 107 72 126 <br /> urr Toluene-d8 991 10 99 71 128 <br /> Surr 4-Bromofluorobenzene 9 6 10 96 76 121 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID D IHPCHEMIMS091DATAI031106103110607 D Batch ID MS9W1106A Analysis Date 11/06/2003 11 16 <br /> Sample ID 03110544-01AMS Units Ng/L Run lD GC/MSD-9_031106A Prep Date 11/06/2003 <br /> Analyte Result PQL SpkVal SpkReNal %REC Lowl-imit HighLimit RPD Ref Val °/aRPD Qua] <br /> Benzene 448 1 3 50 0 90 59 145 <br /> Toluene 436 1 3 50 0 87 39 161 <br /> Ethylbenzene 46 2 13 50 0 92 57 145 <br /> m p-Xylene 922 1 3 100 0 92 37 163 <br /> o-Xylene 46 4 1 3 50 0 93 47 156 <br /> Surr 1,2-Dichloroethane-d4 538 50 108 72 126 <br /> Surr Toluene-d8 489 50 98 71 128 <br /> Surr 4-Bromofluorobenzene 469 50 94 76 121 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B <br /> File ID D IHPCHEMIMS09IDATA1031106103110608 D Batch ID MS9W1106A Analysis Date 11/06/2003 11 40 <br /> Sample ID 03110544-01AMSD Units pg/L Run ID GC/MSO_9_031106A Prep Date 11/06/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimd RPD Ref Val %RPD Qua[ <br /> Benzene 46 5 1 3 50 0 93 59 145 4477 3 73 <br /> Toluene 459 1 3 50 0 92 39 161 4361 509 <br /> Ethylbenzene 491 1 3 50 0 98 57 145 46 15 626 <br /> m p-Xylene 98 3 1 3 100 0 98 37 163 92 16 649 <br /> o-Xylene 49 1 3 50 0 98 47 156 4638 551 <br /> Surr 1,2-Dichloroethane-d4 54 50 108 72 126 <br /> Surr Toluene-d8 487 50 97 71 128 <br /> Surr 4-Bromofluorobenzene 476 50 95 76 121 <br /> Vments <br /> ulations are based off of raw(non-rounded)data However,far reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated <br /> values may differ slightly <br />