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Alpha Analytical, Inc. <br /> 255 Glendale Ave •Suite 21 • Sparks,Nevada 89431-5778 <br /> (775) 355-1044 •(775)355-0406 FAX• 1-800-283-1183 <br /> ate QC Summary Report Work Order <br /> Au 03 43081144 <br /> Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID D 1HPCHEMkMSIOkDATA1030812103081207 D Batch ID MSIOWOB12A Analysis Date 0811212003 09 28 <br /> Sample ID MBLK MS10W0812A Units pgIL Run ID GCIMSD_10_030B12A Prep Date 0811212003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> Tertiary Butyl Alcohol(TBA) NO 5 <br /> Methyl tert-butyl ether(MTBE) NO 0 5 <br /> Di-isopropyl Ether(DIPE) ND I <br /> Ethyl Tertiary Butyl Ether(ETBE) NO 1 <br /> Benzene ND 0 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND I <br /> Toluene NO 0 5 <br /> Ethylbenzene ND 0 5 <br /> m,p-Xylene ND 0 5 <br /> 0-Xylene Na 05 <br /> Surr 1,2-Dichloroethane-d4 108 10 108 72 126 <br /> Surr Toluene-d8 945 10 95 71 128 <br /> Surr 4-Bromofluorobenzene 866 10 87 76 121 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> File ID D 1HPCHEM1MS10kDATAk030B12103081206 D Batch ID MSIOW0812A Analysis Date 08112/2003 09 08 <br /> Sample ID LCS MSIOWOB12A Units pg1L Run ID GCIMSD_10_030812A Prep Date 0811212003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPD Ref Val %RPD Qual <br /> Benzene 933 0 5 10 93 83 119 <br /> Toluene 10 0 5 10 100 80 120 <br /> Ethylbenzene 105 0 5 10 105 80 120 <br /> m,p-Xylene 21 0 5 20 105 77 124 <br /> o-Xylene 978 0 5 10 98 77 125 <br /> er1,2-Dichloroethane-d4 10 10 100 72 126 <br /> r Toluene-d8 103 10 103 71 128 <br /> Surr 4-Bromofluorobenzene 97 10 97 76 121 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID D IHPCHEMkMS101DATA1030812k03081211 D Batch ID MSIOW0812A Analysis Date 08/1212003 10 51 <br /> Sample ID 03081144-02AMS Units pgIL Run ID GCIMSD_10_030812A Prep Date 08112/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual <br /> Benzene 50 1 3 50 0 999 83 119 <br /> Toluene 522 1 3 50 0 104 80 120 <br /> Ethylbenzene 533 1 3 50 0 107 80 120 <br /> m,p-Xylene 105 13 100 0 105 77 124 <br /> o-Xylene 499 1 3 50 0 998 77 125 <br /> Surr 1,2-Dichloroethane-d4 509 50 102 72 126 <br /> Surr Toluene-d8 51 5 50 103 71 128 <br /> Surr 4-Bromofluorobenzene 50 50 999 76 121 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B <br /> File ID D 1HPCHEM%MS101DATX030812103081212 D Batch ID MSIOW0812A Analysis Date 08/12/2003 11 13 <br /> Sample ID 03081144-02AMSD Units pgIL Run ID GCIMSD_10_030812A Prep Date 0811212003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual <br /> Benzene 509 1 3 50 0 102 83 119 4997 175 <br /> Toluene 558 1 3 50 0 112 80 120 5215 673 <br /> Ethylbenzene 532 1 3 50 0 106 80 120 5332 0207 <br /> m,p-Xylene 102 1 3 100 0 102 77 124 1054 333 <br /> o-Xylene 48 1 3 50 0 96 77 125 4989 388 <br /> Surr 1,2-Dichloroethane-d4 503 50 101 72 126 <br /> Surr Toluene-d8 545 50 109 71 128 <br /> Surr 4-Bromofluorobenzene 526 50 105 76 121 <br /> ments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated <br /> S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix <br /> B-Analyte detected in the associated Method Blank <br />