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nacc � oekOrdai <br /> aa-Jur-oo Alpha Analytical, Inc - C Sununar Report <br /> 00053124 <br /> Metnod Blank Test Code SW8015 Batch ID MSBS0527B Analysis Date 06102!2000 19 13 <br /> Sample ID MOLK_00060223 Units mg/Kg Run ID GCIMSDTB 000527 Prep Date 06/0212000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit I )ghl-imit RPD Ref Val %RPD Qual <br /> PH Purgeable ND 1 <br /> Surr 1,2-Dichloroethane-d4 00125 001 125 68 139 <br /> Surr Toluene-d8 000897 001 90 75 127 <br /> Surr 4-Bromofluorobenzene 00116 001 116 73 128 <br /> Laboratory Control Spike Test Code SW8015 Batch ID MS8S052713 Analysis Date 05/29/2000 01 29 <br /> Sample ID GLCS MSBS0527B Units mg/Kg Run ID GCIMSD_8_000527 Prep Date 05129/2000 <br /> Analyte Result PQL SpkVal SpkRefVa1 %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual <br /> TPH Purgeable 761 1 8 95 43 141 <br /> Starr 1 2-Dichloroethane-d4 0 221 02 110 68 139 <br /> Surr Toluene-d8 4 183 02 92 75 127 <br /> Surr 4-Bromofluorobenzene 0 224 02 112 73 128 <br /> Sample Matrix Spike Test Code SW8015 Batch 1D MSBS0527B Analysis Date 05/29/2000 00 12 <br /> Sample ID 00052642-01AGS Units mg/Kg Run ID GC/MSD-8-000527 Prep Date 05/2912000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimt RPD Ref Val %RPD Qual <br /> TPH Purgeable 179 2 16 2054 99 43 141 <br /> Surr 1 2-Dichloroethane-o4 044 04 110 60 139 <br /> Surr Toluene-d8 0 368 04 92 75 127 <br /> Surr 4-Bromofluoroben2ene 0 449 04 112 73 128 <br /> Sample Matrix Spike Duplicate Test Code SW8015 Batch ID MS8S0527B Analysis Date 05129/2000 00 37 <br /> Sample ID 00052642-01AGSD Units mg/Kg Run ID GCIMSD_8_000527 Prep Date 05/29/2000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowbmit Highl-imit RPD Ref Val %RPD Qua] <br /> TPH Purgeable 173 2 16 2054 95 43 141 1789 375 <br /> Surr 1,2-Dichloroethane-d4 0 428 04 107 68 139 <br /> Surr Toluene-d8 037 04 93 75 127 <br /> Surr 4-Bromofluorobenzene 0 451 04 113 73 128 <br /> 5 <br /> Comments Alii-Not Detected at the Reporting Limit D If the spiked value is X25%of the reference value,j ecovery should not be calculated <br /> S-Spike Recovery outside accepted i ecovery limits V-Spike Recovery outside wcepted recovery limits due to matrix <br /> B-Analvte detected to the associated Method Blank <br />